3-(4-氯-2-吡啶)-2,3-二氢-2,2-二甲基-4H-1,3-苯并噁嗪-4-酮合成路线 （共 5 条）
反应条件
hydrogenchloride 8 h; Heating;
参考文献
Wachi, Kazuyuki; Terada, Atsusuke
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 2 p. 465 - 472
反应条件
in chloroform
4 h; Heating;
参考文献
Wachi, Kazuyuki; Terada, Atsusuke
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 2 p. 465 - 472
反应条件
1: 72 percent / PCl5 / POCl3 / 1.) 1 h, rt, 2.) 50 deg C, 2 h
2: 90 percent / CHCl3 / 4 h / Heating
View Scheme
参考文献
Wachi, Kazuyuki; Terada, Atsusuke
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 2 p. 465 - 472
反应条件
1: 20 percent / 1,2-dichloro-ethane / 12 h / Heating
2: 90 percent / CHCl3 / 4 h / Heating
View Scheme
参考文献
Wachi, Kazuyuki; Terada, Atsusuke
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 2 p. 465 - 472
反应条件
in 1,2-dichloro-ethane
12 h; Heating;
参考文献
Wachi, Kazuyuki; Terada, Atsusuke
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 2 p. 465 - 472
