1: para-iodoanisole With tert.-butyl lithium in tetrahydrofuran
T=-78°C; 1 h;
2: With zinc dibromide in tetrahydrofuran
T=20°C; 0.5 h;
3: 1-bromo-2-iodo-benzene With triphenylphosphine; [Pd(dibenzylideneacetone)2] in tetrahydrofuran
T=20°C;
参考文献
Varela, Jesus A.; Pena, Diego; Goldfuss, Bernd; Denisenko, Dmitri; Kulhanek, Jiri; Polborn, Kurt; Knochel, Paul
Chemistry - A European Journal, 2004 , vol. 10, # 17 p. 4252 - 4264
1: 1-bromo-4-methoxy-benzene With tert.-butyl lithium in tetrahydrofuran
T=-78°C; 1 h;
2: With zinc dibromide in tetrahydrofuran
T=-45°C;
3: 1-bromo-2-iodo-benzene With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenylphosphine in tetrahydrofuran
T=20°C; Negishi Coupling;
参考文献
Liesenfeld, Andrea; Lutzen, Arne
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 825 - 831
