4,5-二氧代-4,5-二氢-1H-吡咯[2,3-f]喹啉-2,7,9-三羧酸三甲酯合成路线 （共 37 条）
反应条件
benzoyl t-butyl nitroxide in methanol; chloroform
16 h; Ambient temperature;
参考文献
MacKenzie, A. Roderick; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1983 , # 22 p. 1372 - 1373
反应条件
1: CH2Cl2
2: 21 percent / BBr3 / CH2Cl2
3: 93 percent / tBuN(O)COPh / CH2Cl2; methanol
View Scheme
参考文献
MacKenzie, A. Roderick; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1983 , # 22 p. 1372 - 1373
反应条件
1: CH2Cl2
2: 21 percent / BBr3 / CH2Cl2
3: 93 percent / tBuN(O)COPh / CH2Cl2; methanol
View Scheme
参考文献
MacKenzie, A. Roderick; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1983 , # 22 p. 1372 - 1373
反应条件
1: HCl / methanol / Heating
2: CH2Cl2
3: 21 percent / BBr3 / CH2Cl2
4: 93 percent / tBuN(O)COPh / CH2Cl2; methanol
View Scheme
参考文献
MacKenzie, A. Roderick; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1983 , # 22 p. 1372 - 1373
反应条件
1: xylene / Heating
2: HCl / methanol / Heating
3: CH2Cl2
4: 21 percent / BBr3 / CH2Cl2
5: 93 percent / tBuN(O)COPh / CH2Cl2; methanol
View Scheme
参考文献
MacKenzie, A. Roderick; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1983 , # 22 p. 1372 - 1373
反应条件
1: 21 percent / BBr3 / CH2Cl2
2: 93 percent / tBuN(O)COPh / CH2Cl2; methanol
View Scheme
参考文献
MacKenzie, A. Roderick; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1983 , # 22 p. 1372 - 1373
反应条件
1: NaOMe / methanol / -10 °C
2: xylene / Heating
3: HCl / methanol / Heating
4: CH2Cl2
5: 21 percent / BBr3 / CH2Cl2
6: 93 percent / tBuN(O)COPh / CH2Cl2; methanol
View Scheme
参考文献
MacKenzie, A. Roderick; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1983 , # 22 p. 1372 - 1373
反应条件
1: 62 percent / H2, HCl / 10percent Pd/C / methanol
2: 60 percent / AgO, HNO3 / tetrahydrofuran / 0.17 h / Ambient temperature
View Scheme
参考文献
Gainor, James A.; Weinreb, Steven M.
Journal of Organic Chemistry, 1981 , vol. 46, # 21 p. 4317 - 4319
反应条件
nitric acid in acetic acid
0.5 h; Ambient temperature;
参考文献
Martin, Pierre
Helvetica Chimica Acta, 1993 , vol. 76, # 2 p. 988 - 992
反应条件
1: Br2 / CH2Cl2 / Heating
2: Et3N / diethyl ether / 20 h / 25 °C
3: CH2Cl2 / 7 h / 25 °C
4: dry hydrogen chloride / CH2Cl2 / 10 h
5: 60 percent / ceric ammonium nitrate / acetonitrile; H2O / 0.17 h / 0 °C
View Scheme
参考文献
Corey,E.J.; Tramontano,A.
Journal of the American Chemical Society, 1981 , vol. 103, p. 5599
