in neat (no solvent) byproducts: Et2Se, ethane, ethene; (argon); 45-65°C (upon heating to 80-85°C, the title compd. disappears and Et2Se2 is formed additionally); removal of volatiles (vac.), recrystn. (heptane); elem. anal.;
Clar; Wright
Nature (London, United Kingdom), 1949 , vol. 163, p. 921
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Clar
Chemische Berichte, 1949 , vol. 82, p. 495,514
Journal of the Chemical Society, 1949 , p. 2440
Godchot; Cauquil
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1936 , vol. 202, p. 326
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Banks; Hooker; Richard
Journal of Organic Chemistry, 1956 , vol. 21, p. 547,548
phosphorus pentoxide in neat (no solvent) treatment of SeO2 with HCl at 110-120°C; distn. (three times) over P2O5;; fractional distn. (three times) at about 8 torr while passing of a stream of dry air through the liquid;;
参考文献
Gmelin Handbook: Se: MVol.B, 60, page 133 - 136
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Lenher, V.
Patent: AU1382920 , 1920 ;
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Lenher, V.
Patent: AU1382922 , 1920 ;
