5-(4-氯苯基)-3-噻二唑-1,2,4-噻二唑合成路线 (共 2 条)
反应条件
O-(2,4,6-trimethylbenzenesulfonyl)hydroxylamine in dichloromethane 1) 0 deg C, 1-2 min, 2) room temperature, 2h;
参考文献
Lin, Yang-i; Lang, S. A.; Petty, Sharon R.
Journal of Organic Chemistry, 1980 , vol. 45, # 19 p. 3750 - 3753
反应条件
1: 91 percent / Ambient temperature 2: 75 percent / O-(mesitylenesulfonyl)hydroxylamine / CH2Cl2 / 1) 0 deg C, 1-2 min, 2) room temperature, 2h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 19 p. 3750 - 3753