N-甲基-N-(三甲基硅基)乙酰胺合成路线 （共 33 条）
参考文献
Frainnet,E.; Duboudin,F.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1966 , vol. 262, p. 1693 - 1696
参考文献
Maringgele,W.; Meller,A.
Chemische Berichte, 1978 , vol. 111, p. 538 - 542
参考文献
Shipov; Kramarova; Murasheva; Korlyukov; Pogozhikh; Tarasenko; Negrebetskii; Yakovlev; Baukov, Yu. I.
Russian Journal of General Chemistry, 2011 , vol. 81, # 12 p. 2428 - 2439
参考文献
Hillyard,R.W. et al.
Journal of Organometallic Chemistry, 1978 , vol. 153, p. 369 - 377
反应条件
sodium hydride in cyclohexane
T=15 - 20°C;
参考文献
Tanabe, Yoo; Misaki, Tomonori; Kurihara, Minoru; Iida, Akira; Nishii, Yoshinori
Chemical Communications, 2002 , # 15 p. 1628 - 1629
反应条件
sodium hydride in N,N-dimethyl-formamide
T=60 - 65°C; 1 h;
参考文献
Iida, Akira; Osada, Jun; Nagase, Ryohei; Misaki, Tomonori; Tanabe, Yoo
Organic Letters, 2007 , vol. 9, # 10 p. 1859 - 1862
反应条件
(i) Et3N, benzene, (ii) H2O; Multistep reaction;
参考文献
Yamamoto,Y.; Kimura,H.
Chemical and Pharmaceutical Bulletin, 1976 , vol. 24, p. 1236 - 1241
反应条件
sodium hydride in cyclohexane
T=15 - 20°C; 1 h;
参考文献
Tanabe, Yoo; Misaki, Tomonori; Kurihara, Minoru; Iida, Akira; Nishii, Yoshinori
Chemical Communications, 2002 , # 15 p. 1628 - 1629
反应条件
sodium hydride in N,N-dimethyl-formamide
T=15 - 20°C; Product distribution; Further Variations:Solvents;
参考文献
Tanabe, Yoo; Misaki, Tomonori; Kurihara, Minoru; Iida, Akira; Nishii, Yoshinori
Chemical Communications, 2002 , # 15 p. 1628 - 1629
反应条件
sodium hydride in N,N-dimethyl-formamide
T=60 - 65°C; 1 h;
参考文献
Iida, Akira; Osada, Jun; Nagase, Ryohei; Misaki, Tomonori; Tanabe, Yoo
Organic Letters, 2007 , vol. 9, # 10 p. 1859 - 1862
