74497-02-2合成路线 （共 11739 条）
反应条件
toluene-4-sulfonic acid
参考文献
Gao, Aihong; Mu, Ying; Zhang, Jingshun; Yao, Wei
European Journal of Inorganic Chemistry, 2009 , # 24 p. 3613 - 3621
反应条件
toluene-4-sulfonic acid in benzene
T=20°C; Dean-StarkRefluxInert atmosphere;
参考文献
Liu, Junpeng; Ma, Haiyan
Dalton Transactions, 2014 , vol. 43, # 24 p. 9098 - 9110
反应条件
2: diluted sulfuric acid
View Scheme
参考文献
Semper; Lichtenstadt
Justus Liebigs Annalen der Chemie, 1913 , vol. 400, p. 328
反应条件
Iron (III) nitrate nonahydrate; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; potassium hydroxide in toluene
T=80°C; 36 h; Green chemistry;
参考文献
Zhang, Erlei; Tian, Haiwen; Xu, Sendong; Yu, Xiaochun; Xu, Qing
Organic Letters, 2013 , vol. 15, # 11 p. 2704 - 2707
反应条件
TiO2 nanotubes
T=20°C; 48 h; Neat (no solvent)Sunlight;
参考文献
Hosseini-Sarvari, Mona
Chinese Chemical Letters, 2011 , vol. 22, # 5 p. 547 - 550
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; copper(ll) bromide in water; acetonitrile
T=45°C; P=760.051 Torr; 18 h;
参考文献
Hu, Zhenzhong; Kerton, Francesca M.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 8 p. 1618 - 1624
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Toyoda, Tatsuo; Sasakura, Kazuyuki; Sugasawa, Tsutomu
Tetrahedron Letters, 1980 , vol. 21, p. 173 - 176
反应条件
Iron (III) nitrate nonahydrate; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; potassium hydroxide in toluene
T=80°C; 36 h; Green chemistry;
参考文献
Zhang, Erlei; Tian, Haiwen; Xu, Sendong; Yu, Xiaochun; Xu, Qing
Organic Letters, 2013 , vol. 15, # 11 p. 2704 - 2707
反应条件
in ethyl lactate; water
T=20°C; 0.0833333 h;
参考文献
Bennett, Jacqueline S.; Charles, Kaitlyn L.; Miner, Matthew R.; Heuberger, Caitlin F.; Spina, Elijah J.; Bartels, Michael F.; Foreman, Taylor
Green Chemistry, 2009 , vol. 11, # 2 p. 166 - 168
反应条件
1: 51 percent / polyphosphoric acid / 2 h / 150 °C
2: 88 percent / phosphorus oxybromide / 2 h / 150 °C
3: 88 percent / butyllithium; diisopropylamine / tetrahydrofuran; hexane / 2 h / -75 °C
View Scheme
参考文献
Marull, Marc; Schlosser, Manfred
European Journal of Organic Chemistry, 2003 , # 8 p. 1576 - 1588
