74497-02-2合成路线 （共 11739 条）
参考文献
Masias, A.; Otazo, E.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 591 - 594
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 4 p. 681 - 685
反应条件
1: ammonium thiocyanate; 4-chloro-benzoyl chloride in acetone
T=20°C; 0.166667 h;
2: aniline in acetone
0.166667 h; Heating; Further stages.;
参考文献
Otazo-Sanchez, Elena; Perez-Marin, Leonel; Estevez-Hernandez, Osvaldo; Rojas-Lima, Susana; Alonso-Chamarro, Julian
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 11 p. 2211 - 2218
反应条件
1: ammonium thiocyanate; 4-methoxy-benzoyl chloride in acetone
T=30°C; 0.166667 h;
2: aniline in acetone
0.166667 h; Heating; Further stages.;
参考文献
Otazo-Sanchez, Elena; Perez-Marin, Leonel; Estevez-Hernandez, Osvaldo; Rojas-Lima, Susana; Alonso-Chamarro, Julian
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 11 p. 2211 - 2218
参考文献
Masias, A.; Otazo, E.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 591 - 594
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 4 p. 681 - 685
参考文献
Dixon
Journal of the Chemical Society, 1899 , vol. 75, p. 392
反应条件
sodium hydroxide; water
versetzt die klare Loesung mit 10 ccm Dimethylsulfat;
参考文献
Ullmann
Justus Liebigs Annalen der Chemie, 1903 , vol. 327, p. 110
反应条件
anschl. mit Dimethylsulfat;
参考文献
Ullmann
Justus Liebigs Annalen der Chemie, 1903 , vol. 327, p. 110
反应条件
1: 0.35 g / 1 N NaOH / dioxane / 72 h / Ambient temperature
2: 51 percent / CH2Cl2 / 2 h / Ambient temperature
3: 1.43 g / AcOH, AcONa.3H2O, H2O, 7percent NaHCO3, HCl / dioxane / 3.5 h / 100 °C
View Scheme
参考文献
Ono, Machiko; Tamura, Shinzo
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1453 - 1462
反应条件
in methanol
Yield given;
参考文献
Morita, Tsuyoshi; Okamoto, Yoshiki; Sakurai, Hiroshi
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 1 p. 267 - 273
反应条件
1: water
2: fuming sulfuric acid
View Scheme
参考文献
Hentschel
Chemische Berichte, 1885 , vol. 18, p. 979
Journal fuer Praktische Chemie (Leipzig), 1886 , vol. <2> 34, p. 423
