74497-02-2合成路线 （共 11739 条）
反应条件
T=140 - 150°C; bei der Einwirkung auf salzsaures Anilin;
参考文献
Fischer,O.; Fischer,G.
Chemische Berichte, 1891 , vol. 24, p. 728
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Fischer,O.; Roser
Justus Liebigs Annalen der Chemie, 1881 , vol. 206, p. 155
参考文献
Schering-Kahlbaum A.G.
Patent: DE514248 , 1927 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 2341
参考文献
Zincke; Frohneberg
Chemische Berichte, 1910 , vol. 43, p. 840
参考文献
Zincke; Frohneberg
Chemische Berichte, 1909 , vol. 42, p. 2722 Anm.
Chemische Berichte, 1910 , vol. 43, p. 840
反应条件
in N,N-dimethyl-formamide
参考文献
Krutak,J.J. et al.
Journal of Organic Chemistry, 1979 , vol. 44, p. 3847 - 3858
反应条件
1: 91 percent / xylene / 6 h / Heating
2: 91 percent / NaBH4 / methanol / 0.5 h / Ambient temperature
View Scheme
参考文献
Maroni, Pierre; Cazaux, Louis; Tisnes, Pierre; Zambeti,Marianthie
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 3-4 p. 179 - 186
反应条件
1: hydrogen chloride; concentrated hydrochloric acid
2: diethyl ether / 100 °C / im Rohr
View Scheme
参考文献
Beyer
Journal fuer Praktische Chemie (Leipzig), 1886 , vol. <2> 33, p. 416
反应条件
sodium hypochlorite; tetra(n-butyl)ammonium hydrogensulfate
T=120°C; 12 h;
参考文献
Liang, Jun; Lv, Jing; Shang, Zhi-Cai
Tetrahedron, 2011 , vol. 67, # 44 p. 8532 - 8535
反应条件
1: aniline With n-butyllithium in tetrahydrofuran; hexane
T=-78 - 20°C; Inert atmosphere;
2: 2,4-di-(chloro)-benzaldehyde With YCl3 in toluene
T=20°C; Cannizzaro reaction; 48 h; Inert atmosphere;
3: With hydrogenchloride in water; toluene
T=20°C; Inert atmosphere;
参考文献
Zhang, Lijun; Su, Shunpeng; Wu, Hongping; Wang, Shaowu
Tetrahedron, 2009 , vol. 65, # 48 p. 10022 - 10024
反应条件
in ethanol
Acylation; 1 h; Heating;
参考文献
Dutta, Babul C.; Borthakur, Susanta K.; Goswami, Birendra N.
Journal of the Indian Chemical Society, 1999 , vol. 76, # 11-12 p. 565 - 568
