74497-02-2合成路线 （共 11739 条）
反应条件
2: NO2, O3, O2 / CHCl3 / 1.5 h / 0 °C
View Scheme
参考文献
Suzuki, Hitomi; Tatsumi, Atsuo; Ishibashi, Taro; Mori, Tadashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 4 p. 339 - 344
反应条件
1,3-disulfonic acid imidazolium hydrogen sulfate in neat (no solvent)
T=20°C; 0.0833333 h; Green chemistry; chemoselective reaction;
参考文献
Shirini, Farhad; Khaligh, Nader Ghaffari
Journal of Molecular Liquids, 2013 , vol. 177, p. 386 - 393
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine
Substitution; Heating;
参考文献
Yaguchi, Kyoko; Endo, Yasuyuki
Tetrahedron Letters, 1999 , vol. 40, # 41 p. 7351 - 7354
反应条件
1: potassium tert-butylate; tris-(dibenzylideneacetone)dipalladium(0); bis[2-(diphenylphosphino)phenyl] ether / toluene / 100 °C / |Inert atmosphere
2: palladium diacetate; p-benozquinone; silver(l) oxide / tert-butyl alcohol / 4 h / 80 - 90 °C
View Scheme
参考文献
Chu, Jean-Ho; Huang, Hao-Ping; Hsu, Wen-Ting; Chen, Shih-Tien; Wu, Ming-Jung
Organometallics, 2014 , vol. 33, # 5 p. 1190 - 1204
反应条件
1: potassium tert-butylate; tris-(dibenzylideneacetone)dipalladium(0); bis[2-(diphenylphosphino)phenyl] ether / toluene / 100 °C / |Inert atmosphere
2: palladium diacetate; copper diacetate; p-benozquinone / N,N-dimethyl-formamide / 4 h / 80 - 90 °C
View Scheme
参考文献
Chu, Jean-Ho; Huang, Hao-Ping; Hsu, Wen-Ting; Chen, Shih-Tien; Wu, Ming-Jung
Organometallics, 2014 , vol. 33, # 5 p. 1190 - 1204
反应条件
1: benzene / 5 h / Ambient temperature
2: 5 percent / 50percent aq. NaOH / Duolite A-109 / CH2Cl2 / 70 h / Ambient temperature
View Scheme
参考文献
Harris, Stephen J.; Kinahan, Audrey M.; Meegan, Mary J.; Prendergast, Rhona C.
Journal of Chemical Research, Miniprint, 1994 , # 9 p. 1832 - 1845
参考文献
Ito, Masato; Ootsuka, Takashi; Watari, Ryo; Shiibashi, Akira; Himizu, Akio; Ikariya, Takao
Journal of the American Chemical Society, 2011 , vol. 133, # 12 p. 4240 - 4242
反应条件
in methanol
T=20°C; 0.0833333 h; ultrasound irradiation;
参考文献
Prasad, J. Venkata; Reddy, J. Satyanarayana; Kumar, N. Ravi; Solomon, K. Anand; Gopikrishna
Journal of Chemical Sciences, 2011 , vol. 123, # 5 p. 673 - 679
反应条件
in diphenylether
T=250°C; 15 h;
参考文献
Asherson, Janet L.; Bilgic, Orhan; Young, Douglas W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 522 - 528
反应条件
in diphenylether
T=250°C; 15 h;
参考文献
Asherson, Janet L.; Bilgic, Orhan; Young, Douglas W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 522 - 528
