74497-02-2合成路线 (共 11739 条)
反应条件
2-picoline; Na2S2O5; sulfur dioxide; zinc in N,N-dimethyl-formamide T=20°C; P=2250.2 - 3750.3 Torr; 2 h; other alkylating reagents, other method, other pressure, temp.; various substrates; Product distribution;
参考文献
Wakselman, Claude; Tordeux, Marc
Journal of the Chemical Society, Chemical Communications, 1987 , p. 1701 - 1703
反应条件
in N,N-dimethyl-formamide T=80°C; 5 h; Title compound not separated from byproducts;
参考文献
Umemoto; Ishihara
Tetrahedron Letters, 1990 , vol. 31, # 25 p. 3579 - 3582
反应条件
in N,N-dimethyl-formamide 0.5 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Umemoto; Ishihara
Tetrahedron Letters, 1990 , vol. 31, # 25 p. 3579 - 3582
反应条件
in N,N-dimethyl-formamide T=80°C; 6 h; Inert atmosphere;
参考文献
Mace, Yohan; Raymondeau, Benoit; Pradet, Charlotte; Blazejewski, Jean-Claude; Magnier, Emmanuel
European Journal of Organic Chemistry, 2009 , # 9 p. 1390 - 1397
反应条件
in N,N-dimethyl-formamide T=80°C; 6 h; Inert atmosphere;
参考文献
Mace, Yohan; Raymondeau, Benoit; Pradet, Charlotte; Blazejewski, Jean-Claude; Magnier, Emmanuel
European Journal of Organic Chemistry, 2009 , # 9 p. 1390 - 1397
反应条件
in N,N-dimethyl-formamide T=80°C; 6 h; Inert atmosphere;
参考文献
Mace, Yohan; Raymondeau, Benoit; Pradet, Charlotte; Blazejewski, Jean-Claude; Magnier, Emmanuel
European Journal of Organic Chemistry, 2009 , # 9 p. 1390 - 1397
反应条件
in N,N-dimethyl-formamide T=140°C; 60 h; Title compound not separated from byproducts;
参考文献
Naumann, D.; Pazenok, S. V.; Turra, V.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 1.2 p. 128 - 130
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 1 p. 152 - 155
反应条件
in tetrahydrofuran 10 h; Heating;
参考文献
Yang, Jing-Jing; Kirchmeier, Robert L.; Shreeve, Jean'ne M.
Journal of Organic Chemistry, 1998 , vol. 63, # 8 p. 2656 - 2660
反应条件
in N,N-dimethyl-formamide 20 h; Ambient temperature;
参考文献
Umemoto; Ishihara
Tetrahedron Letters, 1990 , vol. 31, # 25 p. 3579 - 3582
反应条件
in N,N-dimethyl-formamide 0.5 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Umemoto; Ishihara
Tetrahedron Letters, 1990 , vol. 31, # 25 p. 3579 - 3582