74497-02-2合成路线 （共 11739 条）
反应条件
2: (CH3)2S*BH3 / tetrahydrofuran / 24 h / Ambient temperature; THF*BH3
View Scheme
参考文献
Wierenga, Wendell; Griffin, John; Warpehoski, Martha A.
Tetrahedron Letters, 1983 , vol. 24, # 24 p. 2437 - 2440
反应条件
sodium tetrahydroborate; 1-n-butyl-3-methylimidazolium tetrafluoroborate in water
T=20°C; 3 h;
参考文献
Nagaiah; Kumar, V. Naveen; Rao, R. Srinivasa; Reddy; Narsaiah; Yadav
Synthetic Communications, 2006 , vol. 36, # 22 p. 3345 - 3352
反应条件
1: toluene-4-sulfonic acid / ethanol / 0.5 h / |Reflux
2: sodium tetrahydroborate; ethanol / 18 h / 0 - 20 °C
View Scheme
参考文献
Woo, L. W. Lawrence; Wood, Paul M.; Bubert, Christian; Thomas, Mark P.; Purohit, Atul; Potter, Barry V. L.
ChemMedChem, 2013 , vol. 8, # 5 p. 779 - 799
反应条件
T=100 - 110°C; Hantzsch reaction; 0.0583333 h; microwave irradiation;
参考文献
Kidwai; Mohan
Canadian Journal of Chemistry, 2004 , vol. 82, # 3 p. 427 - 429
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=10 - 20°C; 3 h;
参考文献
KUMIAI CHEMICAL INDUSTRY CO., LTD.; IHARA CHEMICAL INDUSTRY CO., LTD.
Patent: EP1982978 A1, 2008 ;
Location in patent: Page/Page column 82 ;
反应条件
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) in toluene
T=60°C; P=760.051 Torr; 6 h;
参考文献
Zhang, Zhenhua; Liu, Yiyang; Ling, Lin; Li, Yuxue; Dong, Yian; Gong, Mingxing; Zhao, Xiaokun; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2011 , vol. 133, # 12 p. 4330 - 4341
反应条件
triethylamine in chloroform
T=61°C; 168 h;
参考文献
Nishiwaki, Nagatoshi; Nishida, Daisei; Ohnishi, Tetsuya; Hidaka, Fumie; Shimizu, Satoru; Tamura, Mina; Hori, Kazushige; Tohda, Yasuo; Ariga, Masahiro
Journal of Organic Chemistry, 2003 , vol. 68, # 22 p. 8650 - 8656
反应条件
4-(N,N-dimethlyamino)pyridine; bis-triphenylphosphine-palladium(II) chloride; triethylamine in water; toluene
UV-irradiationAutoclave;
参考文献
Sumino, Shuhei; Fusano, Akira; Fukuyama, Takahide; Ryu, Ilhyong
Synlett, 2012 , vol. 23, # 9 p. 1331 - 1334
反应条件
in dichloromethane
T=40°C; 24 h;
参考文献
Nakaike, Yumi; Taba, Noriko; Itoh, Shinobu; Tobe, Yoshito; Nishiwaki, Nagatoshi; Ariga, Masahiro
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 12 p. 2413 - 2417
参考文献
Chakraborty, Kajal; Devakumar
Journal of Agricultural and Food Chemistry, 2006 , vol. 54, # 18 p. 6800 - 6808
