74497-02-2合成路线 （共 11739 条）
参考文献
Achmatowicz,O. et al.
Roczniki Chemii, 1965 , vol. 39, p. 1443 - 1446
参考文献
Goodrich Co.
Patent: US2806051 , 1955 ;
反应条件
1: dichloromethane / 2 h / 0 - 20 °C 2: AlCl3, aluminium chloride / 3 h / 120 °C 3: N-bromosuccinmide / N,N-dimethyl-formamide / 12 h / 0 - 20 °C View Scheme
参考文献
WO2012/148808 A1, ;
WO 2012/148808 A1
反应条件
1.1: 1,10-phenanthroline; copper(l) chloride; potassium hydroxide / anhydrous xylene / 72 h / 140 °C / Inert atmosphere 2.1: trichlorophosphate / 48 h / 0 - 120 °C / Inert atmosphere 2.2: 20 °C / Inert atmosphere; Cooling with ice View Scheme
参考文献
He, Ze; Kan, Chi-Wai; Ho, Cheuk-Lam; Wong, Wai-Yeung; Chui, Chung-Hin; Tong, Ka-Lap; So, Shu-Kong; Lee, Tik-Ho; Leung, Louis M.; Lin, Zhenyang
Dyes and Pigments, 2011 , vol. 88, # 3 p. 333 - 343
参考文献
Knoll and Co.
Patent: DE241853 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 10, p. 180
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Knoevenagel
Journal fuer Praktische Chemie (Leipzig), 1914 , vol. <2>89, p. 45
参考文献
Kym
Chemische Berichte, 1890 , vol. 23, p. 425
反应条件
1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 - 5 °C 1.2: 0 - 20 °C 2.1: CuSO4‵5H2O; sodium L-ascorbate / water; tert-butyl alcohol / 20 °C / Darkness 3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 20 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 17 p. 5988 - 5999
反应条件
1: 75 percent / cesium carbonate; Cu(PPh3)3Br / toluene / 24 h / 110 °C 2: 54 percent / cesium carbonate; Cu(PPh3)3Br / toluene / 24 h / 120 °C View Scheme
参考文献
Gujadhur, Rattan; Venkataraman; Kintigh, Jeremy T
Tetrahedron Letters, 2001 , vol. 42, # 29 p. 4791 - 4793
反应条件
T=225°C; microwave irradiation;
参考文献
Glenn, Anne G.; Jones, Paul B.
Tetrahedron Letters, 2004 , vol. 45, # 37 p. 6967 - 6969
反应条件
palladium diacetate; triethylamine; triphenylphosphine in N,N-dimethyl-formamide T=50°C; P=750.075 Torr; 48 h; chemoselective reaction;
参考文献
Marosvoelgyi-Hasko, Diana; Takacs, Attila; Riedl, Zsuzsanna; Kollar, Laszlo
Tetrahedron, 2011 , vol. 67, # 5 p. 1036 - 1040
