74497-02-2合成路线 （共 11739 条）
反应条件
potassium carbonate Inert atmosphere;
参考文献
Kuninobu, Yoichiro; Nishi, Mitsumi; Takai, Kazuhiko
Chemical Communications, 2010 , vol. 46, # 46 p. 8860 - 8862
反应条件
C36H81Cl3P3Ru T=180°C; Yield given. Yields of byproduct given;
参考文献
Tsuji, Yasushi; Yokoyama, Yasuharu; Huh, Keun-Tae; Watanabe, Yoshihisa
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3456 - 3458
反应条件
T=240°C; P=51485.6 Torr;
参考文献
Olsen; Furst
Journal of the American Chemical Society, 1953 , vol. 75, p. 3026
反应条件
Shvo catalyst in 1,1-dimethylpropan-1-ol T=150°C; 24 h; Product distribution; SolventsTemperaturesmol ratioFurther Variations:;
参考文献
Hollmann, Dirk; Baehn, Sebastian; Tillack, Annegret; Parton, Rudy; Altink, Rinke; Beller, Matthias
Tetrahedron Letters, 2008 , vol. 49, # 40 p. 5742 - 5745
反应条件
1: triethylamine / dichloromethane / 0 - 20 °C 2: [RuIII(2,4-pentanedionato)3]; 1,1,1-tris (diphenylphosphinomethyl)ethane; methanesulfonic acid; hydrogen / tetrahydrofuran / 16 h / 200 °C / 7500.75 Torr / |Autoclave; |Inert atmosphere View Scheme
参考文献
Coetzee, Jacorien; Dodds, Deborah L.; Klankermayer, Juergen; Brosinski, Sandra; Leitner, Walter; Slawin, Alexandra M. Z.; Cole-Hamilton, David J.
Chemistry - A European Journal, 2013 , vol. 19, # 33 p. 11039 - 11050
参考文献
Liu, Wei; Ma, Yuan; Yin, Yingwu; Zhao, Yufen
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 4 p. 577 - 579
反应条件
bis-trimethylsilyl ether; phosphorus pentoxide 1) CH2Cl2, 30 min, reflux 2) 160 deg C, 5 h; Yield given. Multistep reaction;
参考文献
Kakimoto, Masa-aki; Ogata, Shin-ichi; Mochizuki, Amane; Imai, Yoshio
Chemistry Letters, 1984 , p. 821 - 824
反应条件
1.1: triethylamine / dichloromethane / 20 °C 2.1: cesium fluoride / toluene; acetonitrile / 48 h / 110 °C / Inert atmosphere; Sealed vial 2.2: 0.33 h / 20 °C View Scheme
参考文献
Pirali, Tracey; Zhang, Fengzhi; Miller, Anna H.; Head, Jenna L.; McAusland, Donald; Greaney, Michael F.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 4 p. 1006 - 1009
参考文献
Gopinath, Vadiraj S.; Pinjari, Jakir; Dere, Ravindra T.; Verma, Aditya; Vishwakarma, Preeti; Shivahare, Rahul; Moger, Manjunath; Kumar Goud, Palusa Sanath; Ramanathan, Vikram; Bose, Prosenjit; Rao; Gupta, Suman; Puri, Sunil K.; Launay, Delphine; Martin, Denis
European Journal of Medicinal Chemistry, 2013 , vol. 69, p. 527 - 536
反应条件
2: 240 °C View Scheme
参考文献
Nandha Kumar; Suresh; Mohan
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 9 p. 2069 - 2073
