74497-02-2合成路线 (共 11739 条)
反应条件
in dichloromethane 12 h; Heating;
参考文献
El Kharrat, Salem; Skander, Myriem; Dahmani, Abdelkader; Laurent, Philippe; Blancou, Hubert
Journal of Organic Chemistry, 2005 , vol. 70, # 21 p. 8327 - 8331
反应条件
in acetic acid T=120°C; cyclocondensation; 8 h;
参考文献
Wang, Quan-Fu; Mao, Yun-Yu; Qin, Chao-Yue; Zhu, Shi-Zheng; Hu, Chang-Ming
Monatshefte fur Chemie, 2000 , vol. 131, # 1 p. 55 - 63
反应条件
1: 86 percent / CH2Cl2 / 2 h / 20 °C 2: acetic acid / 1,2-dichloro-ethane / 6 h / 80 °C View Scheme
参考文献
Linderman; Kirollos
Tetrahedron Letters, 1990 , vol. 31, # 19 p. 2689 - 2692
反应条件
in acetic acid T=120°C; cyclocondensation; 8 h;
参考文献
Wang, Quan-Fu; Mao, Yun-Yu; Qin, Chao-Yue; Zhu, Shi-Zheng; Hu, Chang-Ming
Monatshefte fur Chemie, 2000 , vol. 131, # 1 p. 55 - 63
反应条件
zinc(II) chloride T=255 - 258°C; 21 h;
参考文献
Polish Journal of Chemistry, , vol. 57, # 4/5/6 p. 593 - 596
反应条件
zinc(II) chloride T=240°C;
反应条件
sodium hydroxide; dipotassium peroxodisulfate in water other aromatic amines, ortho-para ratio of products;
参考文献
Behrman, E. J.
Journal of Organic Chemistry, 1992 , vol. 57, # 8 p. 2266 - 2270
反应条件
1: tris-(dibenzylideneacetone)dipalladium(0); 1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate / toluene / 24 h / 80 °C / Inert atmosphere 2: tris-(dibenzylideneacetone)dipalladium(0); 1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate / toluene / 90 °C / Inert atmosphere View Scheme
参考文献
Lim, Younhee; Park, Young-Seo; Kang, Yerang; Jang, Do Young; Kim, Joo Hyun; Kim, Jang-Joo; Sellinger, Alan; Yoon, Do Y.
Journal of the American Chemical Society, 2011 , vol. 133, # 5 p. 1375 - 1382
参考文献
Ullmann; Sane
Chemische Berichte, 1911 , vol. 44, p. 3734
反应条件
1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / 0 °C 2: 70 percent aq. sulfuric acid / 2 h / 60 °C 3: 89 percent / phosphoryl trichloride / 0.5 h / Heating 4: 84 percent / hydrogen, triethylamine / palladium 10 percent on charcoal / ethanol / 4 h / 25 °C View Scheme
参考文献
Shi, Guo-qiang; Takagishi, Sadahito; Schlosser, Manfred
Tetrahedron, 1994 , vol. 50, # 4 p. 1129 - 1134