74497-02-2合成路线 (共 11739 条)
反应条件
trifluorormethanesulfonic acid in dichloromethane T=20°C; 0.0833333 h;
参考文献
Zhao, Yu-Long; Zhang, Wei; Wang, Shuang; Liu, Qun
Journal of Organic Chemistry, 2007 , vol. 72, # 13 p. 4985 - 4988
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate in acetic acid T=25°C; 15 h;
参考文献
Singh, Serjinder; Singh, Iqbal
Journal of the Chemical Society, Chemical Communications, 1982 , # 17 p. 1000 - 1001
参考文献
Sueda, Takuya; Kajishima, Daisuke; Goto, Satoru
Journal of Organic Chemistry, 2003 , vol. 68, # 8 p. 3307 - 3310
反应条件
hydrogen; (ethylenedinitrilo)tetraacetic acid disodium salt; iron(II) sulfate in water T=150°C; P=20686.5 Torr; 12 h; Title compound not separated from byproducts.;
参考文献
Tetrahedron Letters, , vol. 49, # 6 p. 965 - 969
反应条件
1H-imidazole; iodine; chloro-diphenylphosphine in dichloromethane 3 h; Reflux;
参考文献
Nowrouzi, Najmeh; Jonaghani, Mohammad Zareh
Canadian Journal of Chemistry, 2012 , vol. 90, # 6 p. 498 - 509
反应条件
[{(η5-C5Me5)IrCl}2(μ-Cl)2]; potassium carbonate in toluene T=110°C; 24 h; Inert atmosphere;
参考文献
Fristrup, Peter; Tursky, Matyas; Madsen, Robert
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 13 p. 2569 - 2577
反应条件
1: / anhydrous xylene / 1 h / 130 °C / |Inert atmosphere 2: hydrogen; / anhydrous xylene / 130 °C / 750.08 Torr View Scheme
参考文献
Santoro, Federica; Psaro, Rinaldo; Ravasio, Nicoletta; Zaccheria, Federica
RSC Advances, 2014 , vol. 4, # 6 p. 2596 - 2600
反应条件
1: triethylamine / dichloromethane / 0 - 20 °C 2: [RuIII(2,4-pentanedionato)3]; 1,1,1-tris (diphenylphosphinomethyl)ethane; methanesulfonic acid; hydrogen / tetrahydrofuran / 16 h / 200 °C / 7500.75 Torr / |Autoclave; |Inert atmosphere View Scheme
参考文献
Coetzee, Jacorien; Dodds, Deborah L.; Klankermayer, Juergen; Brosinski, Sandra; Leitner, Walter; Slawin, Alexandra M. Z.; Cole-Hamilton, David J.
Chemistry - A European Journal, 2013 , vol. 19, # 33 p. 11039 - 11050
参考文献
Fritsch
Justus Liebigs Annalen der Chemie, 1901 , vol. 315, p. 140 Anm.
反应条件
in nitrobenzene T=40°C; Rate constantMechanism;
参考文献
Shpan'ko, I. V.; Korostylev, A. P.; Rusu, L. N.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1715 - 1723
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 9 p. 1881 - 1888