74497-02-2合成路线 (共 11739 条)
反应条件
1: benzene / Heating 2: Na, DMF / 24 h / 30 °C View Scheme
参考文献
Paventi, Martino; Hay, Allan S.
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5875 - 5882
反应条件
sodium azide; iron(III) chloride adsorbed on silica gel in neat (no solvent) T=45°C; 2 h; SonicationGreen chemistry; Temperature;
参考文献
Habibi, Davood; Mostafaee, Samaneh; Mehrabi, Leila
Journal of Chemical Research, 2013 , vol. 37, # 8 p. 464 - 466
反应条件
indium trifluoromethanesulfonate; sodium azide T=100°C; 2 h; Neat (no solvent);
参考文献
Kundu, Dhiman; Majee, Adinath; Hajra, Alakananda
Tetrahedron Letters, 2009 , vol. 50, # 22 p. 2668 - 2670
反应条件
in 1,4-dioxane T=70°C; 1.5 h;
参考文献
Tetrahedron Letters, , vol. 40, # 12 p. 2327 - 2330
Tetrahedron, , vol. 64, # 16 p. 3589 - 3595
反应条件
in 1,4-dioxane T=100°C; 0.8 h;
参考文献
Tetrahedron, , vol. 64, # 16 p. 3589 - 3595
反应条件
in 1,4-dioxane T=90°C; 12 h;
参考文献
Tetrahedron, , vol. 64, # 16 p. 3589 - 3595
反应条件
sodium azide in acetic acid Heating; Yield given;
参考文献
Gaponik, P. N.; Grigor'ev, Yu. V.; Karavai, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 4 p. 477 - 478
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , vol. 21, # 4 p. 566 - 567
反应条件
T=75°C; Gomberg-Bachman Arylation; regioselective reaction;
参考文献
Chemistry--A European Journal, , vol. 18, # 37 p. 11555 - 11559,5
Chemistry - A European Journal, , vol. 18, # 37 p. 11555 - 11559
参考文献
Quincke
Chemische Berichte, 1888 , vol. 21, p. 1460
反应条件
triethylamine in dichloromethane T=25°C; 16 h; Inert atmosphereIndustry scaleCooling with ice;
参考文献
US2012/316204 A1, ;
Page/Page column 7-8 ;