74497-02-2合成路线 (共 11739 条)
反应条件
(Ru2(η5-C5Ph4O)2(H)2(CO)4) in 1,1-dimethylpropan-1-ol T=150°C; Inert atmosphere;
参考文献
Hollmann, Dirk; Baehn, Sebastian; Tillack, Annegret; Beller, Matthias
Chemical Communications, 2008 , # 27 p. 3199 - 3201
反应条件
palladium 10 on activated carbon in toluene T=175°C; 1.5 h; Inert atmosphereMicrowave irradiation;
参考文献
Lubinu, M. Caterina; De Luca, Lidia; Giacomelli, Giampaolo; Porcheddu, Andrea
Chemistry - A European Journal, 2011 , vol. 17, # 1 p. 82 - 85
参考文献
Hollmann, Dirk; Baehn, Sebastian; Tillack, Annegret; Beller, Matthias
Chemical Communications, 2008 , # 27 p. 3199 - 3201
反应条件
formic acid; C28H28Cl2O3PRuS in toluene T=150°C; 16 h; Inert atmosphere; chemoselective reaction;
参考文献
Sahli, Zeyneb; Sundararaju, Basker; Achard, Mathieu; Bruneau, Christian
Organic Letters, 2011 , vol. 13, # 15 p. 3964 - 3967
反应条件
hydrogen; (ethylenedinitrilo)tetraacetic acid disodium salt; iron(II) sulfate in water T=150°C; P=20686.5 Torr; 12 h; Title compound not separated from byproducts.;
参考文献
Bhor, Malhari D.; Bhanushali, Mayur J.; Nandurkar, Nitin S.; Bhanage, Bhalchandra M.
Tetrahedron Letters, 2008 , vol. 49, # 6 p. 965 - 969
反应条件
LnCl3*6H2O in N,N-dimethyl-formamide 0.166667 h;
参考文献
Bulgakov; Kuleshov; Makhmutov; Dzhemilev
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 10 p. 1573 - 1575
反应条件
tetra-(n-butyl)-phosphonium bromide; PtBr2; phosphorous acid trimethyl ester T=150°C; 10 h; AutoclaveInert atmosphere; Catalytic behavior; regioselective reaction;
参考文献
Rodriguez-Zubiri, Mireia; Anguille, Stephane; Brunet, Jean-Jacques; Daran, Jean-Claude
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 379, p. 103 - 111
参考文献
Hollmann, Dirk; Baehn, Sebastian; Tillack, Annegret; Beller, Matthias
Chemical Communications, 2008 , # 27 p. 3199 - 3201
反应条件
1: With Ti(N(CH3)2)2(C6H5CONC6H3(CH(CH3)2)2)2 in benzene T=20°C; 24 h; Schlenk techniqueInert atmosphereSealed tube; 2: With sodium cyanoborohydride; zinc(II) chloride in methanol T=20°C; 24 h; Inert atmosphere; Overall yield = 62 percent; regioselective reaction;
参考文献
Yim, Jacky C.-H.; Bexrud, Jason A.; Ayinla, Rashidat O.; Leitch, David C.; Schafer, Laurel L.
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 2015 - 2028
反应条件
palladium on magnesium oxide in trifluorotoluene T=180°C; 24 h; AutoclaveInert atmosphere;
参考文献
Corma, Avelino; Rodenas, Tania; Sabater, Maria J.
Chemistry - A European Journal, 2010 , vol. 16, # 1 p. 254 - 260