74497-02-2合成路线 (共 11739 条)
反应条件
potassium fluoride; ethylene glycol
参考文献
Fukui et al.
Kogyo Kagaku Zasshi, 1959 , vol. 62, p. 531,533
Chem.Abstr., 1962 , vol. 57, # 8466
参考文献
Hickinbottom
Journal of the Chemical Society, 1937 , p. 1119,1124
反应条件
rhodium trichloride 3-hydrate; iodine; tetra-n-butylphosphonium iodide; triphenylphosphine T=150°C; 10 h; AutoclaveInert atmosphere; Catalytic behavior; Reagent/catalyst;
参考文献
Rodriguez-Zubiri, Mireia; Baudequin, Christine; Bethegnies, Aurelien; Brunet, Jean-Jacques
Collection of Czechoslovak Chemical Communications, 2012 , vol. 77, # 6 p. 445 - 454
反应条件
potassium hydroxide; tributyl-amine; water; tin(IV) chloride 1.) chlorobenzene, -50 to 80 deg C, 2.) chlorobenzene, THF, reflux; Multistep reaction;
参考文献
Yamaguchi, Masahiko; Arisawa, Mieko; Hirama, Masahiro
Chemical Communications, 1998 , # 13 p. 1399 - 1400
反应条件
1: methanol / 7 h / 40 °C 2: diphenylether / 0.5 h / |Reflux 3: trichlorophosphate / 3 h / |Reflux 4: hydrazine hydrate / |Reflux View Scheme
参考文献
Luo, Wei; Liu, Yang; Wang, Jian; Guo, Chun; Lu, Wei-Qiang; Cui, Kun-Qiang
Medicinal Chemistry Research, 2012 , vol. 21, # 10 p. 3073 - 3079,7
参考文献
Ruegheimer; Hankel
Chemische Berichte, 1896 , vol. 29, p. 2174
反应条件
3: diluted sulfuric acid View Scheme
参考文献
Nietzki
Chemische Berichte, 1884 , vol. 17, p. 345
反应条件
anschl. Kochen mit verd. H2SO4;
参考文献
Nietzki
Chemische Berichte, 1884 , vol. 17, p. 345
Full Text Show Details
Willstaetter; Benz
Chemische Berichte, 1906 , vol. 39, p. 3496
Chemische Berichte, 1907 , vol. 40, p. 1578
反应条件
in ethyl acetate T=90°C; 4 h; Microwave irradiation;
参考文献
Cabrera-Rivera, Fanny A.; Ortiz-Nava, Claudia; Roman-Bravo, Perla; Escalante, Jaime; Leyva, Marco A.
Heterocycles, 2012 , vol. 85, # 9 p. 2173 - 2195,23
反应条件
(1S)-10-camphorsulfonic acid in methanol T=25°C; 24 h; Inert atmosphere;
参考文献
Kumar, K. Siva; Kumar, P. Mahesh; Kumar, K. Anil; Sreenivasulu; Jafar, Ahamed A.; Rambabu; Krishna, G. Rama; Reddy, C. Malla; Kapavarapu, Ravikumar; Shivakumar; Priya, K. Krishna; Parsa, Kishore V. L.; Pal, Manojit
Chemical Communications, 2011 , vol. 47, # 17 p. 5010 - 5012