74497-02-2合成路线 （共 11739 条）
反应条件
N-(chloromethylene)-N-methylmethanaminium chloride; potassium nitrate in neat (no solvent) T=100°C; P=1500.15 Torr; Microwave irradiation; Reagent/catalystTemperature;
参考文献
Kumar, M. Satish; Reddy, K. Rajendar; Rajanna; Venkanna; Krishnaiah
Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2013 , vol. 43, # 8 p. 977 - 983
反应条件
sodium nitrate; sulfuric acid T=0 - 5°C; 3 h;
参考文献
Australian Journal of Chemistry, , vol. 38, # 5 p. 723 - 733
反应条件
1: With tert-butyl methyl ether; nitric acid in tetrahydrofuran T=0°C; 2: With sulfuric acid in dichloromethane T=0°C; 1 h; Further stages. Title compound not separated from byproducts.;
参考文献
Zhang, Pingsheng; Cedilote, Miall; Cleary, Thomas P.; Pierce, Michael E.
Tetrahedron Letters, 2007 , vol. 48, # 49 p. 8659 - 8664
反应条件
sulfuric acid unter Kuehlung;
参考文献
Davis; Blanchard
Journal of the American Chemical Society, 1929 , vol. 51, p. 1804
参考文献
Matsumura, Eizo; Ariga, Masahiro; Tohda, Yasuo; Kawashima, Toshihide
Tetrahedron Letters, 1981 , vol. 22, p. 757 - 758
反应条件
in sulfuric acid below 0°C;
参考文献
Gmelin Handbook: N: MVol.4, 7.7, page 1006 - 1013
参考文献
Plazek; Ropuszynski
Roczniki Chemii, 1959 , vol. 33, p. 397,401
Chem.Abstr., 1960 , p. 350
参考文献
Lesser
Patent: DE148874 ;
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Tingle; Rolker
Journal of the American Chemical Society, 1908 , vol. 30, p. 1890
反应条件
chloroform; dinitrogen tetraoxide
参考文献
Schorygin; Toptschijew
Zhurnal Obshchei Khimii, 1938 , vol. 8, p. 986,988
Chem. Zentralbl., 1939 , vol. 110, # I p. 2174
反应条件
T=120 - 130°C; Man behandelt die Schmelze zur Entfernung von ueberschuessigem Anilin und etwas 2-Nitro-anilin mit Wasserdampf und gewinnt aus dem Rueckstand durch Auskochen mit Wasser;
参考文献
Lesser
Patent: DE148874 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 7, p. 65
