74497-02-2合成路线 （共 11739 条）
反应条件
in ethanol
dithiocarboxylation; 1.5 h; Heating;
参考文献
Mohanta, Pramod K.; Dhar, Sanchita; Samal; Ila; Junjappa
Tetrahedron, 2000 , vol. 56, # 4 p. 629 - 637
反应条件
1: carbon disulfide; aniline With sodium hydroxide in dimethyl sulfoxide
1 h;
2: dimethyl sulfate 2 h;
参考文献
Alagarsamy; Raja Solomon; Dhanabal
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 1 p. 235 - 241
反应条件
acetic acid
16 h; Reflux;
参考文献
Yu, Chao-Wu; Chang, Pei-Teh; Hsin, Ling-Wei; Chern, Ji-Wang
Journal of Medicinal Chemistry, 2013 , vol. 56, # 17 p. 6775 - 6791
反应条件
phosphorus trichoride
1.) 1,2-dichlorobenzene; 2.) reflux; Yield given. Multistep reaction;
参考文献
Clemence; Joliveau-Maushart; Meier; et al.
European Journal of Medicinal Chemistry, 1985 , vol. 20, # 3 p. 257 - 266
反应条件
1: 77 percent / triethylamine / benzene / 5 h / Heating
2: 68 percent / CHCl3 / 6 h / Heating
3: 87 percent / hydrazine hydrate, triethylamine / ethanol / 10 h / Heating
View Scheme
参考文献
Previtera; Basile; Monforte; Pizzimenti
Farmaco, Edizione Scientifica, 1987 , vol. 42, # 10 p. 735 - 745
反应条件
in N,N-dimethyl-formamide
T=135°C; 0.05 h; microwave irradiation;
参考文献
Arya, Kapil; Agarwal, Manish
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 1 p. 86 - 93
参考文献
Abd El-Nabi, Hisham A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 2 p. 211 - 214
反应条件
trichlorophosphate
T=100°C;
参考文献
Ziegler; Gelfert
Monatshefte fuer Chemie, 1959 , vol. 90, p. 822,825
Monatshefte fuer Chemie, 1959 , vol. 90, p. 858,862
反应条件
1: 230 - 240 °C
2: aluminium chloride / 140 °C
View Scheme
参考文献
Gao, Wen-Tao; Hou, Wen-Duan; Zheng, Mei-Ru; Tang, Li-Jun
Synthetic Communications, 2010 , vol. 40, # 5 p. 732 - 738
反应条件
in N,N-dimethyl-formamide
T=20°C;
参考文献
Gondela, Andrzej; Walczak, Krzysztof
Tetrahedron, 2007 , vol. 63, # 13 p. 2859 - 2864
