74497-02-2合成路线 （共 11739 条）
反应条件
1: 20 °C
2: 86 percent / iodine; zinc / dioxane / 0.08 h / 20 °C / sonication
View Scheme
参考文献
Ross, Nathan A.; MacGregor, Robert R.; Bartsch, Richard A.
Tetrahedron, 2004 , vol. 60, # 9 p. 2035 - 2041
反应条件
1: 20 °C
2: 72 percent / iodine; zinc / dioxane / 0.08 h / 20 °C / sonication
View Scheme
参考文献
Ross, Nathan A.; MacGregor, Robert R.; Bartsch, Richard A.
Tetrahedron, 2004 , vol. 60, # 9 p. 2035 - 2041
反应条件
5A molecular sieve in benzene
72 h;
参考文献
Buchanan, Gerald W.; Morin, Frederick G.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 530 - 536
反应条件
1.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C
2.1: boron trifluoride diethyl etherate / m-xylene / -78 - 20 °C
2.2: 17 h / 190 °C / |Autoclave
3.1: hydrogenchloride; sodium nitrite / water / 0.17 h / 0 - 5 °C
3.2: 1 h / 20 °C
4.1: 2-methyl-2-iodopropane / dichloromethane / 18 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Maury, Julien; Feray, Laurence; Bertrand, Michele P.; Kapat, Ajoy; Renaud, Philippe
Tetrahedron, 2012 , vol. 68, # 47 p. 9606 - 9611,6
参考文献
Matsumura, Eizo; Ariga, Masahiro; Tohda, Yasuo; Kawashima, Toshihide
Tetrahedron Letters, 1981 , vol. 22, p. 757 - 758
反应条件
[Emim][Gly] in ethanol
T=20°C; Michael Addition; 5 h; Catalytic behavior; TemperatureTimeSolvent; stereoselective reaction;
参考文献
Morimoto, Naoki; Takeuchi, Yasuo; Nishina, Yuta
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 368-369, p. 31 - 37
反应条件
iodine in methanol
T=20°C; 0.5 h;
参考文献
Gu, Yanlong; Ogawa, Chikako; Kobayashi, Juta; Mori, Yuichiro; Kobayashi, Shu
Angewandte Chemie - International Edition, 2006 , vol. 45, # 43 p. 7217 - 7220
反应条件
sodium hydroxide in water
T=20°C; 2.4 h; Green chemistry; Reagent/catalystTimeSolvent;
参考文献
Sayin, Serkan; Yilmaz, Mustafa
RSC Advances, 2014 , vol. 4, # 5 p. 2219 - 2225
反应条件
potassium fluoride; natural phosphate in methanol
T=20°C; Michael addition; 1 h;
参考文献
Zahouily, Mohamed; Bahlaouan, Bouchaib; Rayadh, Ahmed; Sebti, Said
Tetrahedron Letters, 2004 , vol. 45, # 21 p. 4135 - 4138
反应条件
aminosulfonic acid in ethanol
T=20°C; Mannich reaction;
参考文献
Luo, Hai-Tang; Kang, Yu-Ru; Nie, Hong-Yun; Yang, Li-Ming
Journal of the Chinese Chemical Society (Taipei, Taiwan), 2009 , vol. 56, # 1 p. 186 - 195
