74497-02-2合成路线 （共 11739 条）
反应条件
1: aniline With hydrogenchloride; sodium nitrite
2: N-(o-fluorobenzylidene)anthranilic acid With acetic acid in ethanol
T=0 - 20°C; pH=3;
参考文献
Kumar, Ashok; Bansal, Deepti; Bajaj, Kiran; Sharma, Shalabh; Archana; Srivastava
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 23 p. 5281 - 5291
反应条件
1: aniline With hydrogenchloride; sodium nitrite
2: N-(p-chlorobenzylidene)anthranilic acid With acetic acid in ethanol
T=0 - 20°C; pH=3;
参考文献
Kumar, Ashok; Bansal, Deepti; Bajaj, Kiran; Sharma, Shalabh; Archana; Srivastava
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 23 p. 5281 - 5291
反应条件
1: aniline With hydrogenchloride; sodium nitrite
2: N-(2,6-dichlorobenzylidene)anthranilic acid With acetic acid in ethanol
T=0 - 20°C; pH=3;
参考文献
Kumar, Ashok; Bansal, Deepti; Bajaj, Kiran; Sharma, Shalabh; Archana; Srivastava
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 23 p. 5281 - 5291
参考文献
Kolinski,R.A. et al.
Roczniki Chemii, 1977 , vol. 51, p. 1365 - 1375
反应条件
HClO4 immobilized on silica in toluene
T=100°C; 5 h; Green chemistry;
参考文献
Kumar, Dinesh; Sonawane, Mukesh; Pujala, Brahmam; Jain, Varun K.; Bhagat, Srikant; Chakraborti, Asit K.
Green Chemistry, 2013 , vol. 15, # 10 p. 2872 - 2884
反应条件
in toluene
16 h; Heating / reflux;
参考文献
SATO PHARMACEUTICAL CO., LTD.
Patent: WO2007/4543 A1, 2007 ;
Location in patent: Page/Page column 19-20 ;
参考文献
Masias, A.; Otazo, E.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 591 - 594
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 4 p. 681 - 685
反应条件
1: ammonium thiocyanate; 4-methyl-benzoyl chloride in acetone
T=30°C; 0.166667 h;
2: aniline in acetone
0.166667 h; Heating; Further stages.;
参考文献
Otazo-Sanchez, Elena; Perez-Marin, Leonel; Estevez-Hernandez, Osvaldo; Rojas-Lima, Susana; Alonso-Chamarro, Julian
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 11 p. 2211 - 2218
参考文献
Boyle, Nicholas A.; Chegwidden, W. Richard; Blackburn, G. Michael
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 2 p. 222 - 224
反应条件
(i) Na2SO3*7H2O, (ii) PCl5, (iii) /BRN= 605631/, benzene; Multistep reaction;
参考文献
Farrar,W.V.
Journal of the Chemical Society, 1960 , p. 3058 - 3062
