74497-02-2合成路线 （共 11739 条）
反应条件
1: pyridine / |Reflux
2: tert.-butylnitrite / acetonitrile / 24 h / 45 °C
View Scheme
参考文献
Kilpatrick, Brenden; Heller, Markus; Arns, Steve
Chemical Communications, 2013 , vol. 49, # 5 p. 514 - 516
反应条件
bei der Einwirkung auf salzsaures Anilin und anschl. Neutralisieren mit NaOH;
参考文献
Kalle and Co
Chem. Zentralbl., 1898 , vol. 69, # II p. 159
Full Text Show Details
Kalle and Co.
Patent: DE96851 ;
反应条件
1: 92 percent / dioxane / Ambient temperature
2: 35 percent / TFA, p-chloranil
View Scheme
参考文献
Hitotsuyanagi, Yukio; Kobayashi, Masatsugu; Fukuyo, Masamoto; Takeya, Koichi; Itokawa, Hideji
Tetrahedron Letters, 1997 , vol. 38, # 48 p. 8295 - 8296
反应条件
in N,N-dimethyl-formamide
Heating;
参考文献
Priimenko, B. A.; Samura, B. A.; Garmash, S. N.; Klyuev, N. A.; Romanenko, N. I.
Pharmaceutical Chemistry Journal, 1983 , vol. 17, # 2 p. 105 - 108
Khimiko-Farmatsevticheskii Zhurnal, 1983 , vol. 17, # 2 p. 160 - 164
反应条件
in ethanol
T=175 - 180°C; 6 h;
参考文献
Garmash, S. N.; Priimenko, B. A.; Klyuev, N. A.; Romanenko, N. I.; Golets, V. A.; Kozik, T. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988 , p. 442 - 445
Khimiya Geterotsiklicheskikh Soedinenii, 1988 , vol. 24, # 4 p. 534 - 537
反应条件
in N,N-dimethyl-formamide
Heating;
参考文献
Priimenko, B. A.; Samura, B. A.; Garmash, S. N.; Klyuev, N. A.; Romanenko, N. I.
Pharmaceutical Chemistry Journal, 1983 , vol. 17, # 2 p. 105 - 108
Khimiko-Farmatsevticheskii Zhurnal, 1983 , vol. 17, # 2 p. 160 - 164
反应条件
sodium lauryl sulfate in water
T=20°C; Mannich reaction; 10 h; Micellar solution;
参考文献
Jafari, Abbas Ali; Moradgholi, Fatemeh; Tamaddon, Fatemeh
European Journal of Organic Chemistry, 2009 , # 8 p. 1249 - 1255
反应条件
[Emim][Gly] in ethanol
T=20°C; Michael Addition; 48 h;
参考文献
Morimoto, Naoki; Takeuchi, Yasuo; Nishina, Yuta
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 368-369, p. 31 - 37
反应条件
Yb(OSO2C8H17)3 in toluene
T=60°C; Mannich-type reaction; 12 h;
参考文献
Yi, Wen-Bin; Cai, Chun
Journal of Fluorine Chemistry, 2006 , vol. 127, # 11 p. 1515 - 1521
反应条件
iron(III) chloride in dichloromethane
T=-70 - 0°C;
参考文献
Fuks, R.; Caillaux, B.; Hanocq, M.; Bril, M. Van den
Synthetic Communications, 1983 , vol. 13, # 3 p. 265 - 268
