74497-02-2合成路线 （共 11739 条）
反应条件
(i) NaNO2, aq. HCl, (ii) /BRN= 956618/, NaOAc*3H2O; Multistep reaction;
参考文献
Weingarten,H.
Journal of Organic Chemistry, 1961 , vol. 26, p. 730 - 733
反应条件
1: 94 percent / KOH; Pd[P(t-Bu3)]2; cetyltrimethylammonium bromide / toluene; H2O / 3 h / 90 °C 2: 98 percent / KOH; Pd[P(t-Bu3)]2; cetyltrimethylammonium bromide / toluene; H2O / 6 h / 90 °C View Scheme
参考文献
Gujadhur, Rattan; Venkataraman; Kintigh, Jeremy T
Tetrahedron Letters, 2001 , vol. 42, # 29 p. 4791 - 4793
反应条件
hydrogenchloride; sodium nitrite 1. H2O, 0 deg C; 2. 0 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Slouka, Jan; Bekarek, Vojtech
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 5 p. 1379 - 1387
反应条件
zinc(II) chloride T=240°C;
参考文献
Galewski, Zbigniew
Molecular Crystals and Liquid Crystals (1969-1991), 1987 , vol. 151, p. 233 - 242
反应条件
2: cobalt (II)-chloride / 212 °C View Scheme
参考文献
Hickinbottom
Journal of the Chemical Society, 1937 , p. 1119,1124
反应条件
1: 87 percent / 96percent NaOH / 72 h / 100 °C 2: 83 percent / pyridine / CH2Cl2 / 24 h / Heating 3: 1.) POCl3 / 1.) ice bath cooling, 30 min, 2.) 90 deg C, 2 h View Scheme
参考文献
Moon; Shim; Lee
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 1994 , vol. 247, p. 91 - 97
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1007 - 1014
参考文献
Curtius; Haas
Journal fuer Praktische Chemie (Leipzig), 1921 , vol. <2>102, p. 111
反应条件
1: F2; TfOH / 20 °C 2: F2; TfOH / 20 °C 3: F2; TfOH / 20 °C View Scheme
参考文献
Alric; Marquet; Billard; Langlois
Journal of Fluorine Chemistry, 2005 , vol. 126, # 4 p. 661 - 667
反应条件
1: water; hydrochloric acid / und Behandeln des Reaktionsprodukts mit konz. Schwefelsaeure und Acetanhydrid 2: phosphoryl chloride View Scheme
参考文献
Bangdiwala; Desai
Journal of the Indian Chemical Society, 1954 , vol. 31, p. 43,46
