74497-02-2合成路线 (共 11739 条)
反应条件
in 1,4-dioxane
Heating;
参考文献
Arseniyadis, Simeon; Gore, Jacques
Tetrahedron Letters, 1983 , vol. 24, # 37 p. 3997 - 4000
参考文献
Atherton; Lambert
Tetrahedron, 1983 , vol. 39, # 15 p. 2599 - 2608
反应条件
2: acetone / 9 h / Heating
View Scheme
参考文献
Atherton; Lambert
Tetrahedron, 1983 , vol. 39, # 15 p. 2599 - 2608
反应条件
2: acetone / 9 h / Heating
3: hydrazine, conc. HCl / ethanol / 5 h / Heating
4: 86 percent / conc. HCl, NaNO2, K2CO3 / H2O / 4.5 h
View Scheme
参考文献
Atherton; Lambert
Tetrahedron, 1983 , vol. 39, # 15 p. 2599 - 2608
反应条件
1: 9 percent / 3.5 h / 160 °C
2: NaNO2, HCl / H2O
View Scheme
参考文献
Atherton; Lambert
Tetrahedron, 1983 , vol. 39, # 15 p. 2599 - 2608
反应条件
1: 9 percent / 3.5 h / 160 °C
2: NaNO2, HCl / H2O
View Scheme
参考文献
Atherton; Lambert
Tetrahedron, 1983 , vol. 39, # 15 p. 2599 - 2608
反应条件
1: pyridine / CH2Cl2 / 1) 1 h, 0 deg C; 2) 1 h, 25 deg C
2: 83 percent / NaH / dimethylformamide / 110 °C
View Scheme
参考文献
Wager, Carrie A. B.; Miller, Sandra A.
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 7 p. 615 - 622
反应条件
1: pyridine / CH2Cl2 / 1) 1 h, 0 deg C; 2) 1 h, 25 deg C
2: 61 percent / NaH / dimethylformamide / 110 °C
View Scheme
参考文献
Sundberg, Richard J.; Laurino, Joseph P.
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 249 - 254
参考文献
Jones; Kenner
Journal of the Chemical Society, 1933 , p. 363,366
反应条件
bis-(benzothiazol-2-yl)-disulphide; triethylamine; triphenylphosphine in dichloromethane; N,N-dimethyl-formamide
3 h; Ambient temperature;
参考文献
Ito, Kazuo; Iida, Toshiyuki; Fujita, Takako; Tsuji, Satoshi
Synthesis, 1981 , # 4 p. 287