74497-02-2合成路线 （共 11739 条）
反应条件
1: 38 percent / sodium hydroxide / H2O; ethyl acetate / 0.75 h / 10 - 20 °C
2: N-methylpyrrolidine / tetrahydrofuran / 72 h / 55 °C
View Scheme
参考文献
Braverman; Cherkinsky; Kedrova; Reiselman
Tetrahedron Letters, 1999 , vol. 40, # 16 p. 3235 - 3238
反应条件
methanol; sulfur
T=100°C; unter Druck;
参考文献
Monsanto Chem. Co.
Patent: US2857430 , 1956 ;
反应条件
phosphorus trichoride in acetonitrile
T=20 - 50°C;
参考文献
Giri, Ramesh; Lam, Jonathan K.; Yu, Jin-Quan
Journal of the American Chemical Society, 2010 , vol. 132, # 2 p. 686 - 693
反应条件
1: copper powder / 70 - 85 °C
2: beim Benzoylieren und Behandeln mit alkoh. Salzsaeure bei 20grad
View Scheme
参考文献
Wang, Huamin; Cao, Xiangxiang; Xiao, Fuhong; Liu, Saiwen; Deng, Guo-Jun
Organic Letters, 2013 , vol. 15, # 18 p. 4900 - 4903
反应条件
1-n-butyl-3-methylimidazolium tetrafluoroborate
T=20°C; 0.166667 h; Ionic liquidSonication;
参考文献
Pawar, Omprakash B.; Chavan, Fulchand R.; Sakate, Sachin S.; Shinde, Narayan D.
Chinese Journal of Chemistry, 2010 , vol. 28, # 1 p. 69 - 71
反应条件
aluminium trichloride; silica gel; zinc(II) chloride
0.1 h; microwave irradiation;
参考文献
Dabiri, Minoo; Salehi, Peyman; Mohammadi, Ali A.; Baghbanzadeh, Mostafa
Synthetic Communications, 2005 , vol. 35, # 2 p. 279 - 287
反应条件
iodine; acetic acid in water; acetonitrile
7 h; Reflux;
参考文献
Dabiri, Minoo; Salehi, Peyman; Bahramnejad, Mahboobeh; Alizadeh, Mohsen
Monatshefte fur Chemie, 2010 , vol. 141, # 8 p. 877 - 881
反应条件
toluene-4-sulfonic acid
0.1 h; microwave irradiation;
参考文献
Dabiri, Minoo; Salehi, Peyman; Khajavi, Mohammad S.; Mohammadi, Ali A.
Heterocycles, 2004 , vol. 63, # 6 p. 1417 - 1421
反应条件
acetic acid
4 h; Reflux;
参考文献
Tiwari, Ravi; Chhabra, Gurmeet
Asian Journal of Chemistry, 2010 , vol. 22, # 8 p. 5981 - 5986
反应条件
toluene-4-sulfonic acid
Irradiation;
参考文献
Rad-Moghadam, Kurosh; Khajavi, Mohammad S.
Journal of Chemical Research - Part S, 1998 , # 11 p. 702 - 703
