74497-02-2合成路线 （共 11739 条）
反应条件
boron trifluoride diethyl etherate; mercury(II) oxide
参考文献
Air Reduction Co.
Patent: US2703333 , 1954 ;
参考文献
Bergmann et al.
Recueil des Travaux Chimiques des Pays-Bas, 1952 , vol. 71, p. 168,192
Journal of the American Chemical Society, 1953 , vol. 75, p. 358
反应条件
1: triethylamine / acetonitrile / 20 - 30 °C
2: acetonitrile / 4 h / 100 °C
View Scheme
参考文献
Bogolubsky, Andrey V.; Ryabukhin, Sergey V.; Pipko, Sergey E.; Lukin, Oleg; Shivanyuk, Alexander; Mykytenko, Dmytro; Tolmachev, Andrey
Tetrahedron, 2011 , vol. 67, # 20 p. 3619 - 3623
反应条件
1: With hydrogenchloride in ethanol; water
pH=5; Reflux;
2: With sodium hydroxide in ethanol; water
pH=7;
参考文献
Fassihi, Afshin; Abedi, Daryoush; Saghaie, Lotfollah; Sabet, Razieh; Fazeli, Hossein; Bostaki, Ghasem; Deilami, Omid; Sadinpour, Hekmatollah
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 5 p. 2145 - 2157
反应条件
1: 66 percent / 8 h / 120 °C
2: 82 percent / H2 / 10percent Pd/C / ethanol / Ambient temperature
View Scheme
参考文献
Faerber, M.; Osiander, H.; Severin, T.
Journal of Heterocyclic Chemistry, 1994 , vol. 31, # 4 p. 947 - 956
反应条件
potassium tert-butylate; copper(l) iodide; tributylphosphine in toluene
T=135°C; 10.5 h; high pressure;
参考文献
Patil, Nandkumar M.; Kelkar, Ashutosh A.; Nabi, Zahid; Chaudhari, Raghunath V.
Chemical Communications, 2003 , # 19 p. 2460 - 2461
反应条件
copper; potassium carbonate; 18-crown-6 ether in 1,2-dichloro-benzene
15 h; Heating;
参考文献
Gauthier, Sylvie; Frechet, Jean M. J.
Synthesis, 1987 , # 4 p. 383 - 385
参考文献
Zincke; Weisspfenning
Journal fuer Praktische Chemie (Leipzig), 1912 , vol. <2>85, p. 208
参考文献
Zincke; Weisspfenning
Journal fuer Praktische Chemie (Leipzig), 1912 , vol. <2>85, p. 208
参考文献
Reitzenstein; Rothschild
Journal fuer Praktische Chemie (Leipzig), 1906 , vol. <2> 73, p. 269
Full Text Show Details
Zincke; Weispfenning
Journal fuer Praktische Chemie (Leipzig), 1910 , vol. <2> 82, p. 2,7, 9
