N,N'-(亚甲基二-4,1-亚苯基)二-氨基甲酸 C,C'-二甲基酯合成路线 （共 10 条）
反应条件
N-trimethyl-butyltetrafluoroboric acid; zinc oxide T=200 - 240°C; P=48.7549 Torr; 2.66667 h;
参考文献
LANZHOU INSTITUTE OF CHEMICAL PHYSICS, CHINESE ACADEMY OF SCIENCES
Patent: US2011/21810 A1, 2011 ;
Location in patent: Page/Page column 4 ;
反应条件
montmorillonite K-10 in decalin T=190°C; 5 h;
参考文献
Uriz, Pedro; Serra, Marc; Salagre, Pilar; Castillon, Sergio; Claver, Carmen; Fernandez, Elena
Tetrahedron Letters, 2002 , vol. 43, # 9 p. 1673 - 1676
反应条件
Zn(CH3COO)2*2H2O
T=180°C; P=6000.6 Torr; 2.66667 h; AutoclaveInert atmosphere; Product distribution / selectivity;
参考文献
Bayer MaterialScience AG
Patent: EP2230228 A1, 2010 ;
Location in patent: Page/Page column 9; 10 ;
反应条件
1,10-phenanthroline; C14H29(C6H13)3P(+)PF6(-); palladium dichloride
T=135°C; P=10343.2 Torr; 24 h;
参考文献
Yang, Qian; Robertson, Al; Alper, Howard
Organic Letters, 2008 , vol. 10, # 21 p. 5079 - 5082
参考文献
Caraculacu, Adrian A.; Agherghinei, Ion; Gaspar, Mariana; Prisacariu, Cristina
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 8 p. 1343 - 1348
反应条件
oxygen; triphenylphosphine; AuCl(PPh3)2
T=200°C; P=37503.8 Torr; 3 h;
参考文献
Shi; Deng
Chemical Communications, 2001 , # 5 p. 443 - 444
反应条件
scandium tris(trifluoromethanesulfonate) in tetrahydrofuran
T=89.85°C; 24 h; Title compound not separated from byproducts;
参考文献
Distaso, Monica; Quaranta, Eugenio
Journal of Catalysis, 2004 , vol. 228, # 1 p. 36 - 42
反应条件
sulfuric acid in water
Heating;
参考文献
Li, Tao; Li, Huiquan; Qin, Guotong; Liu, Haitao; Pei, Yixia
Frontiers of Chemistry in China, 2010 , vol. 5, # 1 p. 99 - 103
反应条件
1: 1.2-dichloro-benzene
View Scheme
参考文献
Siefken
Justus Liebigs Annalen der Chemie, 1949 , vol. 562, p. 75,1114
反应条件
hydrogenchloride; sulfuric acid
T=100°C; 0.25 h; other catalysts; Product distributionMechanism;
参考文献
Jakus, Vladimir; Bojsova, Eva
Collection of Czechoslovak Chemical Communications, 1992 , vol. 57, # 7 p. 1505 - 1515
