反应条件
1.1: sodium hydroxide; water / tetrahydrofuran / 3 h / 50 °C
2.1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 18 h / 25 °C
3.1: triethylamine / toluene / 2 h / -10 °C
4.1: dihydrogen peroxide; lithium hydroxide hydrate / methanol; water / 1 h / -10 °C
4.2: -10 - 20 °C
View Scheme
参考文献
Yamagami, Takafumi; Hatsuda, Masanori; Utsugi, Masayuki; Kobayashi, Ryo; Moritani, Yasunori
European Journal of Organic Chemistry, 2013 , # 33 p. 7467 - 7470
