双(五甲基环戊烯)钴(II)合成路线 （共 7 条）
反应条件
Na#Hg in tetrahydrofuran stirring for 12 h; decantation, evapn., sublimation in vac., crystn. from hexane; elem. anal.;
参考文献
Robbins,J.L.; Edelstein,N.; Spencer,B.
Journal of the American Chemical Society, 1982 , vol. 104, p. 1882
反应条件
in dimethyl sulfoxide Kinetics; rate const. for the electron self-exchange of redox couple , obtained by using the NMR line-broadening technique;
参考文献
Journal of the American Chemical Society, , vol. 110, # 6 p. 1745 - 1749
反应条件
in tetrahydrofuran stirring (20°C, 2 h); evapn., extn. (water, Et2O);
参考文献
Russian Chemical Bulletin, , vol. 45, # 10 p. 2427 - 2430
反应条件
in tetrahydrofuran stirring (20°C, 2 h); evapn., extn. (hexane), chromy. (Al2O3, hexane); elem. anal.;
参考文献
Russian Chemical Bulletin, , vol. 45, # 10 p. 2427 - 2430
反应条件
in tetrahydrofuran stirring (20°C, 2 h); evapn., extn. (water, Et2O), chromy. (Al2O3, hexane), recrystn. (toluene/hexane); elem. anal.;
参考文献
Russian Chemical Bulletin, , vol. 45, # 10 p. 2427 - 2430
反应条件
oxygen in dichloromethane not isolated;
参考文献
Choi, Doo Seong; Kim, Dong Hyun; Shin, Ueon Sang; Deshmukh, Ravindra R.; Lee, Sang-Gi; Song, Choong Eui
Chemical Communications, 2007 , # 33 p. 3467 - 3469
反应条件
in tetrahydrofuran
(N2), added dropwise, cooled at -40°C; filtered, dried in vac., soln. evaporated, diluted with heptane, cooled at -30°C, filtered, dried in vac.; elem. anal., IR;
参考文献
Calderazzo, Fausto; Marchetti, Fabio; Ungari, Fausto; Wieber, Markus
Gazzetta Chimica Italiana, 1991 , vol. 121, # 2 p. 93 - 100
