4-甲氧基苯基氨基甲酸乙酯合成路线 （共 33 条）
反应条件
ammonium hydroxide; iron in methanol
T=25°C; Reduction; condensation; 0.5 h; sonication;
参考文献
Chandrasekhar; Narsihmulu
Tetrahedron Letters, 2000 , vol. 41, # 41 p. 7969 - 7972
反应条件
cBRIDP; bis(η3-allyl-μ-chloropalladium(II)); sodium t-butanolate in water
T=50°C; 24 h; Inert atmosphereGreen chemistry;
参考文献
Isley, Nicholas A.; Dobarco, Sebastian; Lipshutz, Bruce H.
Green Chemistry, 2014 , vol. 16, # 3 p. 1480 - 1488
反应条件
copper(l) iodide; 2-(2,6-dimethylphenyl-amino)-2-oxoacetic acid potassium salt
T=110°C; 24 h; Inert atmosphere;
参考文献
Yang, Xinye; Zhang, Yihua; Ma, Dawei
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2443 - 2446,4
反应条件
pyridine; oxygen; iron; iodine; palladium dichloride
T=180°C; P=30003 Torr; 1 h;
参考文献
Karpinska; Baran; Skupinska
Polish Journal of Chemistry, 2008 , vol. 82, # 5 p. 1105 - 1116
反应条件
[Pt(triphenylphosphine)2Cl2]; tin(IV) chloride; triethylamine
T=180°C; P=45600 Torr; 4 h;
参考文献
Watanabe; Tsuji; Takeuchi; Suzuki
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 11 p. 3343 - 3348
反应条件
sodium hydride in benzene
5 h; Heating;
参考文献
Angeles; Santillan; Martinez; Ramirez; Moreno; Salmon
Synthetic Communications, 1994 , vol. 24, # 17 p. 2441 - 2447
反应条件
N-bromosuccinmide; 1,8-diazabicyclo[5.4.0]undec-7-ene
T=120°C; Hofmann rearrangement; Microfluidic flow;
参考文献
Palmieri, Alessandro; Ley, Steven V.; Hammond, Kelvin; Polyzos, Anastasios; Baxendale, Ian R.
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3287 - 3289
反应条件
1: sodium azide; copper(II) sulfate / methanol / 12 h / 30 °C
2: palladium dichloride; triethylamine / N,N-dimethyl acetamide / 24 h / 70 °C / 760.05 Torr / |Schlenk technique
View Scheme
参考文献
Ren, Long; Jiao, Ning
Chemical Communications, 2014 , vol. 50, # 28 p. 3706 - 3709
参考文献
Whitehead; Traverso
Journal of the American Chemical Society, 1955 , vol. 77, p. 5872,5875
参考文献
Whitehead; Traverso
Journal of the American Chemical Society, 1955 , vol. 77, p. 5872,5875
