反应条件
1: 88 percent / m-chloroperoxybenzoic acid, 4,4'-thiobis-(6-t-butyl-3-methylphenol) / 1,2-dichloro-ethane / 9 h / Ambient temperature
2: H2 / 10percent Pd-C / ethanol / Ambient temperature
3: oxidation with Jones reagent
4: 92 percent / conc. H2SO4 / 0.08 h / 0 °C
View Scheme
参考文献
Pfister, Juerg R.
Tetrahedron Letters, 1980 , vol. 21, p. 1281 - 1284