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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
74601-56-2
合成路线
（共 9 条）
74601-56-2
→
反应条件
74834-03-0
N-[2-[[4-氯-2-(2-氯苯甲酰基)苯基]-甲基氨基]-2-氧代乙基]丁酰胺
反应条件
1: 97 percent / 20percent HBr / acetic acid / 1 h / Ambient temperature 2: 85.6 percent / dimethylformamide / 3.5 h / Ambient temperature View Scheme
参考文献
Hirai, Kentaro; Ishiba, Teruyuki; Sugimoto, Hirohiko; Fujishita, Toshio; Tsukinoki, Yuji; Hirose, Katsumi
Journal of Medicinal Chemistry, 1981 , vol. 24, # 1 p. 20 - 27
74601-56-2
→
反应条件
65808-66-4
2-乙酰氨基-N-[4-氯-2-(2-氯苯甲酰基)苯基]-N-甲基-乙酰胺
反应条件
1: 97 percent / 20percent HBr / acetic acid / 1 h / Ambient temperature 2: 47.4 percent / dimethylformamide / 3.5 h / Ambient temperature View Scheme
参考文献
Hirai, Kentaro; Ishiba, Teruyuki; Sugimoto, Hirohiko; Fujishita, Toshio; Tsukinoki, Yuji; Hirose, Katsumi
Journal of Medicinal Chemistry, 1981 , vol. 24, # 1 p. 20 - 27
74601-56-2
→
反应条件
65808-69-7
反应条件
1: 97 percent / 20percent HBr / acetic acid / 1 h / Ambient temperature 2: 92 percent / dimethylformamide / 3.5 h / Ambient temperature View Scheme
参考文献
Hirai, Kentaro; Ishiba, Teruyuki; Sugimoto, Hirohiko; Fujishita, Toshio; Tsukinoki, Yuji; Hirose, Katsumi
Journal of Medicinal Chemistry, 1981 , vol. 24, # 1 p. 20 - 27
74601-56-2
→
反应条件
65808-72-2
N-[[[4-氯-2-(2-氯苯甲酰基)苯基]-甲基-氨基甲酰]甲基]十六烷酰胺
反应条件
1: 97 percent / 20percent HBr / acetic acid / 1 h / Ambient temperature 2: 45.5 percent / dimethylformamide / 3.5 h / Ambient temperature View Scheme
参考文献
Hirai, Kentaro; Ishiba, Teruyuki; Sugimoto, Hirohiko; Fujishita, Toshio; Tsukinoki, Yuji; Hirose, Katsumi
Journal of Medicinal Chemistry, 1981 , vol. 24, # 1 p. 20 - 27
74601-56-2
→
反应条件
65808-73-3
N-[4-氯-2-(2-氯苯甲酰基)苯基]-N-甲基-2-[(2-苯基乙酰基)氨基]乙酰胺
反应条件
1: 97 percent / 20percent HBr / acetic acid / 1 h / Ambient temperature 2: 85.3 percent / dimethylformamide / 3.5 h / Ambient temperature View Scheme
参考文献
Hirai, Kentaro; Ishiba, Teruyuki; Sugimoto, Hirohiko; Fujishita, Toshio; Tsukinoki, Yuji; Hirose, Katsumi
Journal of Medicinal Chemistry, 1981 , vol. 24, # 1 p. 20 - 27
74601-56-2
→
反应条件
59179-95-2
氯扎封
反应条件
1: 97 percent / 20percent HBr / acetic acid / 1 h / Ambient temperature 2: 93.5 percent / dimethylformamide / 3 h / Ambient temperature 3: 90 percent / NH2NH2*H2O / ethanol / 0.5 h / Heating View Scheme
参考文献
Hirai, Kentaro; Ishiba, Teruyuki; Sugimoto, Hirohiko; Fujishita, Toshio; Tsukinoki, Yuji; Hirose, Katsumi
Journal of Medicinal Chemistry, 1981 , vol. 24, # 1 p. 20 - 27
74601-56-2
→
反应条件
59180-45-9
反应条件
1: 97 percent / 20percent HBr / acetic acid / 1 h / Ambient temperature 2: 89 percent / hexamethylphosphoric acid triamide / 5 h 3: 91.5 percent / KI / acetone / 1 h / Heating 4: 100 percent / ethanol; CHCl3; methanol / 3 h / Ambient temperature View Scheme
参考文献
Hirai, Kentaro; Ishiba, Teruyuki; Sugimoto, Hirohiko; Fujishita, Toshio; Tsukinoki, Yuji; Hirose, Katsumi
Journal of Medicinal Chemistry, 1981 , vol. 24, # 1 p. 20 - 27
74601-56-2
→
反应条件
59180-46-0
反应条件
1: 97 percent / 20percent HBr / acetic acid / 1 h / Ambient temperature 2: 89 percent / hexamethylphosphoric acid triamide / 5 h 3: 91.5 percent / KI / acetone / 1 h / Heating 4: 88.9 percent / ethanol; CHCl3; methanol / 3 h / Ambient temperature View Scheme
参考文献
Hirai, Kentaro; Ishiba, Teruyuki; Sugimoto, Hirohiko; Fujishita, Toshio; Tsukinoki, Yuji; Hirose, Katsumi
Journal of Medicinal Chemistry, 1981 , vol. 24, # 1 p. 20 - 27
74601-56-2
→
反应条件
59180-47-1
反应条件
1: 97 percent / 20percent HBr / acetic acid / 1 h / Ambient temperature 2: 89 percent / hexamethylphosphoric acid triamide / 5 h 3: 91.5 percent / KI / acetone / 1 h / Heating 4: 84.7 percent / ethanol; CHCl3; methanol / 3 h / Ambient temperature View Scheme
参考文献
Hirai, Kentaro; Ishiba, Teruyuki; Sugimoto, Hirohiko; Fujishita, Toshio; Tsukinoki, Yuji; Hirose, Katsumi
Journal of Medicinal Chemistry, 1981 , vol. 24, # 1 p. 20 - 27
