1,3,3a,4,7,7a-六氢-2-苯并噻吩合成路线 （共 4 条）
反应条件
lead(IV) acetate; N-amino-phthalimide in dichloromethane 1 h; Ambient temperature;
参考文献
Aitken, R. Alan; Gosney, Ian; Farries, Hugh; Palmer, Michael H.; Simpson, Isobel; et. al.
Tetrahedron, 1985 , vol. 41, # 7 p. 1329 - 1346
反应条件
sodium sulfide in ethanol; water
12 h; Heating;
参考文献
Aitken, R. Alan; Gosney, Ian; Farries, Hugh; Palmer, Michael H.; Simpson, Isobel; et. al.
Tetrahedron, 1985 , vol. 41, # 7 p. 1329 - 1346
反应条件
1: 75.7 percent / pyridine / 3 h / 0 °C
2: 33.3 percent / Na2S*9H2O / aq. ethanol / 17 h / Heating
View Scheme
参考文献
Mundy,B.P.; Theodore,J.J.
Journal of the American Chemical Society, 1980 , vol. 102, p. 2005
反应条件
1: 75 percent / m-chloroperbenzoic acid / diethyl ether / 60 h / Ambient temperature
2: 94 percent / Br2 / CH2Cl2 / 0.5 h / -78 °C
3: 46 percent / DBU / tetrahydrofuran / 48 h / 45 °C
4: 55 percent / Pd on charcoal / benzene / 15 h / Heating
View Scheme
参考文献
Aitken, R. Alan; Cadogen, J. I. G.; Gosney, Ian; Newlands, Stephen
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 16 p. 2301 - 2308
