4-氯-N,N-二甲基苯磺酰胺合成路线 (共 14 条)
反应条件
1: pyridine 2: LiAlH4 View Scheme
参考文献
Eliel; Nelson
Journal of Organic Chemistry, 1955 , vol. 20, p. 1657,1661
反应条件
1: pyridine 2: aq. NaOH solution View Scheme
参考文献
Journal of Organic Chemistry, , vol. 20, p. 1657,1661
反应条件
ammonium hydroxide T=250°C; P=139746 Torr;
参考文献
Journal of Organic Chemistry, , vol. 20, p. 1657,1661
反应条件
In(OSO2CF3)3 in 1,2-dichloro-ethane
T=100°C; 24 h;
参考文献
Frost, Christopher G.; Hartley, Joseph P.; Griffin, David
Synlett, 2002 , # 11 p. 1928 - 1930
反应条件
aluminum oxide; potassium hydroxide
T=130°C; 0.0666667 h; microwave irradiation;
参考文献
Malik, Sarika; Nadir, Upender K.; Pandey, Pramod S.
Synthetic Communications, 2008 , vol. 38, # 18 p. 3074 - 3081
反应条件
copper diacetate; 3-phenyl-2-propenoic acid; copper(l) chloride
T=110°C; 24 h; Reagent/catalyst;
参考文献
Huang, Xin; Wang, Jichao; Ni, Zhangqin; Wang, Sichang; Pan, Yuanjiang
Chemical Communications, 2014 , vol. 50, # 35 p. 4582 - 4584
反应条件
sodium hydroxide; water
参考文献
Geigy A.G.
Patent: CH248800 , 1945 ;
反应条件
hydrogenchloride; water; copper(l) chloride
Diazotization;
参考文献
Geigy A.G.
Patent: CH246983 , 1945 ;
参考文献
Geigy A.G.
Patent: CH248800 , 1945 ;
反应条件
1: chlorobenzene; sodium carbonate
2: ethanol / Und Erwaermen der Natrium-Salzes mit Dimethylsulfat in Chlorbenzol
View Scheme
参考文献
Geigy A.G.
Patent: CH245679 , 1945 ;