4-(二甲基氨基)乙酰苯胺合成路线 （共 25 条）
反应条件
die Reaktionsprodukte mit Salzsaeure erhitzt;
参考文献
Pinnow; Koch
Chemische Berichte, 1897 , vol. 30, p. 2857 Anm.
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Hoechster Farbw.
Patent: DE88557 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 4, p. 70
反应条件
sulfuric acid; nitric acid T=0°C;
参考文献
Wilshire, John F. K.
Australian Journal of Chemistry, 1982 , vol. 35, # 12 p. 2497 - 2504
参考文献
Hodgson; Crook
Journal of the Chemical Society, 1932 , p. 2976
反应条件
1-propanephosphonic acid cyclic anhydride in tetrahydrofuran; ethyl acetate
T=70°C; Beckmann rearrangement; 0.5 h; Inert atmosphere;
参考文献
Augustine, John Kallikat; Kumar, Rajesha; Bombrun, Agnes; Mandal, Ashis Baran
Tetrahedron Letters, 2011 , vol. 52, # 10 p. 1074 - 1077
反应条件
methanol; hydrogen
T=99.84°C; P=9750.98 Torr; 0.616667 h; Autoclave;
参考文献
Rong, Zeming; Zhang, Wenjun; Zhang, Peng; Sun, Zhuohua; Lv, Jinkun; Du, Wenqiang; Wang, Yue
Catalysis Communications, 2013 , vol. 41, p. 115 - 118
反应条件
pyridine
T=80°C; Acetylation; 0.5 h;
参考文献
Jones II, Guilford; Lu, Lily N.; Fu, Hongning; Farahat, Catie W.; Oh, Churl; Greenfield, Scott R.; Gosztola, David J.; Wasielewski, Michael R.
Journal of Physical Chemistry B, 1999 , vol. 103, # 3 p. 572 - 581
反应条件
zinc(II) tetrahydroborate; zinc(II) chloride in tetrahydrofuran
12 h; Ambient temperature;
参考文献
Bhattacharyya, Sukanta; Chatterjee, Arindam; Duttachowdhury, Shiti, Kantha
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 1 p. 1 - 2
参考文献
Milanesi, Silvia; Fagnoni, Maurizio; Albini, Angelo
Chemical Communications, 2003 , # 2 p. 216 - 217
反应条件
in acetonitrile
T=20°C; 0.166667 h; Irradiation;
参考文献
Dichiarante, Valentina; Fagnoni, Maurizio; Albini, Angelo
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1282 - 1289
反应条件
1: hydroxylamine hydrochloride; sodium acetate / methanol; water / Reflux
2: 1-propanephosphonic acid cyclic anhydride / tetrahydrofuran; ethyl acetate / 0.5 h / 70 °C / Inert atmosphere
View Scheme
参考文献
Augustine, John Kallikat; Kumar, Rajesha; Bombrun, Agnes; Mandal, Ashis Baran
Tetrahedron Letters, 2011 , vol. 52, # 10 p. 1074 - 1077
