2-氨基-1-苯并[1,3]二氧代-5-乙醇合成路线 （共 5 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether
a) 0 deg C, 6 h, b) RT, overnight, c) reflux, 4 h;
参考文献
Makki, Mohamad S. I.; Samarkandy, Abdul-Rahim A.; Kabuli, Rida A.; Hewlins, M. J. E.
Journal of the Indian Chemical Society, 1994 , vol. 71, # 2 p. 75 - 80
反应条件
1: H2O / 0.25 h
2: 3.97 g / LiAlH4 / tetrahydrofuran / 6 h / Ambient temperature
View Scheme
参考文献
Kihara; Ohnishi; Vangveravong; Kobayashi
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 4 p. 870 - 876
反应条件
palladium; acetic acid
Hydrogenation;
参考文献
Kindler; Peschke
Archiv der Pharmazie (Weinheim, Germany), 1931 , vol. 269, p. 581,600
Justus Liebigs Annalen der Chemie, 1935 , vol. 519, p. 291,295
反应条件
ethanol; platinum
Hydrogenation;
参考文献
Reichert; Koch
Chemische Berichte, 1935 , vol. 68, p. 445,450
反应条件
1: potassium acetate; methanol
2: platinum; ethanol / Hydrogenation
View Scheme
参考文献
Reichert; Koch
Chemische Berichte, 1935 , vol. 68, p. 445,450
