2-癸基-1,4,7,10,13-戊氧杂环十五烷合成路线 （共 7 条）
反应条件
sodium hydroxide in diethylene glycol dimethyl ether
T=90 - 120°C; 27 h;
参考文献
Mizuno, Tadashi; Nakatsuji, Yohji; Yanagida, Shozo; Okahara, Mitsuo
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 2 p. 481 - 484
反应条件
1: 74 percent / NBA / 2 h / 45 - 50 °C
2: 30 percent / NaOH / bis-(2-methoxy-ethyl) ether / 27 h / 90 - 120 °C
View Scheme
参考文献
Mizuno, Tadashi; Nakatsuji, Yohji; Yanagida, Shozo; Okahara, Mitsuo
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 2 p. 481 - 484
反应条件
1: 74 percent / NBA / 2 h / 45 - 50 °C
2: 30 percent / NaOH / bis-(2-methoxy-ethyl) ether / 27 h / 90 - 120 °C
View Scheme
参考文献
Mizuno, Tadashi; Nakatsuji, Yohji; Yanagida, Shozo; Okahara, Mitsuo
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 2 p. 481 - 484
反应条件
1: NaH / dioxane / 24 h / Heating
2: p-toluenesulfonyl chloride; NaOH / dioxane
View Scheme
参考文献
Chou, Fang-Fei; Shih, Jeng-Shong
Journal of the Chinese Chemical Society, 2002 , vol. 49, # 4 p. 599 - 605
反应条件
1: NaH / dioxane / 24 h / Heating
2: p-toluenesulfonyl chloride; NaOH / dioxane
View Scheme
参考文献
Chou, Fang-Fei; Shih, Jeng-Shong
Journal of the Chinese Chemical Society, 2002 , vol. 49, # 4 p. 599 - 605
反应条件
sodium methylate
1.) sodium methoxide, dioxane, diol, 10 min 2.) 1,2-bis<2'-(toluene-p-sulphonyloxy)ethoxy>ethane, dioxane, 5 min, reflux; Multistep reaction;
参考文献
Bowsher, Brian R.; Rest, Antony J.; Main, Brian G.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 1421 - 1426
反应条件
Yield given. Multistep reaction;
参考文献
Ikeda, Isao; Yamamura, Shingo; Nakatsuji, Yohji; Okahara, Mitsuo
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5355 - 5358
