2-十二烷基-1,4,7,10,13-戊氧杂环十五烷合成路线 （共 4 条）
反应条件
sodium hydroxide in diethylene glycol dimethyl ether
T=90 - 120°C; 27 h;
参考文献
Mizuno, Tadashi; Nakatsuji, Yohji; Yanagida, Shozo; Okahara, Mitsuo
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 2 p. 481 - 484
反应条件
1: 84 percent / NBS / 2 h / 45 - 50 °C
2: 36 percent / NaOH / bis-(2-methoxy-ethyl) ether / 27 h / 90 - 120 °C
View Scheme
参考文献
Mizuno, Tadashi; Nakatsuji, Yohji; Yanagida, Shozo; Okahara, Mitsuo
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 2 p. 481 - 484
反应条件
1: 84 percent / NBS / 2 h / 45 - 50 °C
2: 36 percent / NaOH / bis-(2-methoxy-ethyl) ether / 27 h / 90 - 120 °C
View Scheme
参考文献
Mizuno, Tadashi; Nakatsuji, Yohji; Yanagida, Shozo; Okahara, Mitsuo
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 2 p. 481 - 484
反应条件
Yield given. Multistep reaction;
参考文献
Ikeda, Isao; Yamamura, Shingo; Nakatsuji, Yohji; Okahara, Mitsuo
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5355 - 5358
