N-(2-氯苯基)-4-甲氧基苯甲酰胺合成路线 （共 6 条）
反应条件
1: para-iodoanisole; 2-chloro-aniline With palladium diacetate; triethylamine in water
0.166667 h;
2: carbon monoxide in water
T=100°C; P=10343.2 Torr; 8 h;
参考文献
Tambade, Pawan J.; Patil, Yogesh P.; Qureshi, Ziyauddin S.; Dhake, Kishor P.; Bhanage, Bhalchandra M.
Synthetic Communications, 2012 , vol. 42, # 2 p. 176 - 185
反应条件
anhydrous iron chloride; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene
T=135°C; 24 h; Inert atmosphere;
参考文献
Correa, Arkaitz; Elmore, Simon; Bolm, Carsten
Chemistry - A European Journal, 2008 , vol. 14, # 12 p. 3527 - 3529
反应条件
lithium diisopropyl amide in tetrahydrofuran
T=-70 - -20°C;
参考文献
Tandel, Sagun; Wang, Anlai; Holdeman, Terra C.; Zhang, Hongming; Biehl, Edward R.
Tetrahedron, 1998 , vol. 54, # 50 p. 15147 - 15154
反应条件
1: BF3(g) / hexane
2: PCl5
View Scheme
参考文献
Auricchio, Sergio; Bini, Antonella; Pastormerlo, Eros; Ricca, Aldo; Truscello, Ada M.
Tetrahedron, 1994 , vol. 50, # 25 p. 7589 - 7596
反应条件
Schotten-Baumann reaction;
参考文献
El-Sheikh, Mustafa I.; Marks, Alan; Biehl, Edward R.
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3256 - 3259
反应条件
(R)-(+)-1,1'-binaphthyl-2,2'-diamine; copper(II) bis(trifluoromethanesulfonate); caesium carbonate in N,N-dimethyl-formamide
T=135°C; Ullmann type intramolecular coupling; 28 h; Inert atmosphere;
参考文献
Naidu, Ajay B.; Sekar, Govindasamy
Synthesis, 2010 , # 4 art. no. Z20609SS, p. 579 - 586
