1-甲氧基-4-(4-甲基-4-戊烯-1-基)苯合成路线 (共 2 条)
反应条件
1: 1-(2-bromoethyl)-4-methoxy-benzene With magnesium in tetrahydrofuran
0.5 h; Heating;
2: 3-chloro-2-methyl-propene in tetrahydrofuran
16 h;
参考文献
Taylor, Stephen K.; Ivanovic, Milica; Simons, Lloyd J.; Davis, Matthew M.
Tetrahedron Asymmetry, 2003 , vol. 14, # 6 p. 743 - 747
反应条件
sulfuric acid
1) benzene, 20 deg C, 66 h; 2) 0 deg C, then 15 h at 80 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lehmkuhl, Herbert; McLane, Raymond
Liebigs Annalen der Chemie, 1980 , # 5 p. 736 - 743