4-甲氧基-3,5-二(2-甲基-2-丙基)苯甲醛合成路线 （共 7 条）
反应条件
water; potassium carbonate
Reflux;
参考文献
Villalonga-Barber, Carolina; Meligova, Aggeliki K.; Alexi, Xanthippi; Steele, Barry R.; Kouzinos, Constantinos E.; Screttas, Constantinos G.; Katsanou, Efrosini S.; Micha-Screttas, Maria; Alexis, Michael N.
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 1 p. 339 - 351
反应条件
1: K2CO3 / 18-crown-6 / acetone; dimethylformamide / 48 h / Heating
2: HCl / acetone / 40 °C
View Scheme
参考文献
Shanahan, Charles S.; McGrath, Dominic V.
Journal of Organic Chemistry, 2005 , vol. 70, # 3 p. 1054 - 1056
反应条件
1: 93 percent / NBS; DMSO
2: p-toluenesulfonic acid / benzene / 48 h / Heating
3: K2CO3 / 18-crown-6 / acetone; dimethylformamide / 48 h / Heating
4: HCl / acetone / 40 °C
View Scheme
参考文献
Shanahan, Charles S.; McGrath, Dominic V.
Journal of Organic Chemistry, 2005 , vol. 70, # 3 p. 1054 - 1056
反应条件
1: p-toluenesulfonic acid / benzene / 48 h / Heating
2: K2CO3 / 18-crown-6 / acetone; dimethylformamide / 48 h / Heating
3: HCl / acetone / 40 °C
View Scheme
参考文献
Shanahan, Charles S.; McGrath, Dominic V.
Journal of Organic Chemistry, 2005 , vol. 70, # 3 p. 1054 - 1056
反应条件
potassium carbonate in acetone
15 h; Heating;
参考文献
Hori, Hitoshi; Nagasawa, Hideko; Ishibashi, Masaki; Uto, Yoshihiro; Hirata, Akihiko; Saijo, Kouichi; Ohkura, Kazuto; Kirk, Kenneth L; Uehara, Yoshimasa
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 10 p. 3257 - 3265
反应条件
1: 98 percent / laccase; oxygen; TEMPO / acidic aq. solution / 24 h / 20 °C / pH 5
2: t-BuOK / acetonitrile / 36 h / 80 °C
View Scheme
参考文献
D'Acunzo, Francesca; Galli, Carlo; Gentili, Patrizia; Sergi, Federica
New Journal of Chemistry, 2006 , vol. 30, # 4 p. 583 - 591
反应条件
methanol; potassium borohydride in tetrahydrofuran
T=50°C; 24 h;
参考文献
D'Acunzo, Francesca; Galli, Carlo; Gentili, Patrizia; Sergi, Federica
New Journal of Chemistry, 2006 , vol. 30, # 4 p. 583 - 591
