1-(叔丁基二甲基硅氧基)-2-丙酮合成路线 （共 14 条）
反应条件
1H-imidazole in N,N-dimethyl-formamide
参考文献
Baldwin, Ian R.; Whitby, Richard J.
Chemical Communications, 2003 , # 22 p. 2786 - 2787
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in water
参考文献
Caldwell, Richard D.; GUCKIAN, Kevin M.; KUMARA VEL, Gnanasambandam; LEE, Wen-Cherng; LIN, Edward Yin-Shiang; LlU, Xiaogao; MA, Bin; SCOTT, Daniel M.; SHl, Zhan; THOMAS, Jermaine; TAVERAS, Arthur G.; ZHENG, Guo Zhu
Patent: US2014/100195 A1, 2014 ;
Location in patent: Page/Page column ;
反应条件
ozone in methanol T=20°C; 4.73333 h;
参考文献
O'Brien, Matthew; Baxendale, Ian R.; Ley, Steven V.
Organic Letters, 2010 , vol. 12, # 7 p. 1596 - 1598
反应条件
lithium aluminium tetrahydride in diethyl ether T=-100 - -10°C;
参考文献
Dalla; Catteau
Tetrahedron, 1999 , vol. 55, # 21 p. 6497 - 6510
反应条件
N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve in dichloromethane Oxidation; 6 h;
参考文献
Koppisch, Andrew T.; Blagg, Brian S. J.; Poulter, C. Dale
Organic Letters, 2000 , vol. 2, # 2 p. 215 - 217
反应条件
dicobalt octacarbonyl T=20°C; P=760.051 Torr; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 25 p. 9630 - 9634
反应条件
in N-methyl-acetamide; water
反应条件
1: 97 percent / N-ethyldiisopropylamine / CH2Cl2 / 16 h / 20 °C 2: 91 percent / TPAP; NMO; 4 Angstroem molecular sieves / CH2Cl2 / 6 h View Scheme
参考文献
Organic Letters, , vol. 2, # 2 p. 215 - 217
反应条件
[(salph)Cr(THF)2][Co(CO)4] in ethylene glycol dimethyl ether T=22°C; P=760 Torr; 6 h; Product distribution; Further Variations:Pressuresreaction times;
参考文献
Organic Letters, , vol. 8, # 17 p. 3709 - 3712
反应条件
1: 73 percent / Et3N / CH2Cl2 / 2 h / Heating 2: 93 percent / LiAlH4 / diethyl ether / -100 - -10 °C View Scheme
参考文献
Tetrahedron, , vol. 55, # 21 p. 6497 - 6510
