3,4-二氢-1-苯基萘合成路线 （共 70 条）
反应条件
1: 3,4-dihydronaphthalene-1(2H)-one With phosphorochloridic acid diphenyl ester; 2,4,6-trimethylphenylmagnesium bromide in tetrahydrofuran
T=0 - 20°C; 1 h;
2: phenyl-magnesium chloride With bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
T=65°C; 0.5 h;
参考文献
Miller, Joseph A.
Tetrahedron Letters, 2002 , vol. 43, # 39 p. 7111 - 7114
反应条件
Ni(PCy3)2Cl2; potassium carbonate; tri-cyclo-hexyl-phosphine in 1,4-dioxane; water
T=110°C; Suzuki-Miyaura coupling; 16 h; Inert atmosphere;
参考文献
Xu, Li; Li, Bi-Jie; Wu, Zhen-Hua; Lu, Xing-Yu; Guan, Bing-Tao; Wang, Bi-Qin; Zhao, Ke-Qing; Shi, Zhang-Jie
Organic Letters, 2010 , vol. 12, # 4 p. 884 - 887
反应条件
zeolite Ca Y in hexane
T=22°C; 0.0833333 h;
参考文献
Pitchumani; Joy, Abraham; Prevost, Nicolette; Ramamurthy
Chemical Communications, 1997 , # 1 p. 127 - 128
反应条件
FeCl3*6H2O in 1,2-dichloro-ethane
T=40°C; 5 h; Inert atmosphere;
参考文献
Dal Zotto, Christophe; Wehbe, Johny; Virieux, David; Campagne, Jean-Marc
Synlett, 2008 , # 13 p. 2033 - 2035
反应条件
bis-triphenylphosphine-palladium(II) chloride; caesium carbonate in N,N-dimethyl acetamide
T=60°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Venkatesh, Varadhachari
European Journal of Organic Chemistry, 2009 , # 25 p. 4300 - 4306
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran
T=20 - 70°C; 1 h;
参考文献
Eom, Dahan; Park, Sangjune; Park, Youngchul; Lee, Kooyeon; Hong, Gilbert; Lee, Phil Ho
European Journal of Organic Chemistry, 2013 , # 13 p. 2672 - 2682
反应条件
potassium phosphate; Ni(PCy3)2Cl2; water in 1,4-dioxane; toluene
T=110°C; Suzuki-Miyaura coupling; 20 h; Inert atmosphere;
参考文献
Sun, Chang-Liang; Yang, Wang; Xiao, Zhou; Wu, Zhen-Hua; Li, Bi-Jie; Guan, Bing-Tao; Shi, Zhang-Jie
Chemistry - A European Journal, 2010 , vol. 16, # 20 p. 5844 - 5847
反应条件
1: phenyllithium With zinc(II) chloride in tetrahydrofuran; anhydrous butyl ether
T=20°C; Negishi coupling reaction;
2: 3,4-dihydronaphthalen-1-yl acetate With Ni(PCy3)2Cl2 in tetrahydrofuran; anhydrous butyl ether; dimethylammonium 2,4-dichlorophenoxyacetate
T=20 - 60°C;
参考文献
Sun, Chang-Liang; Yang, Wang; Xiao, Zhou; Wu, Zhen-Hua; Li, Bi-Jie; Guan, Bing-Tao; Shi, Zhang-Jie
Chemistry - A European Journal, 2010 , vol. 16, # 20 p. 5844 - 5847
反应条件
acetic acid; RhCl(PPh3)3 in toluene
T=90°C; 60 h;
参考文献
Chiusoli, Gian Paolo; Costa, Mirco; Melli, Luca
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 495 - 506
参考文献
Weiss; Woidich
Monatshefte fuer Chemie, 1925 , vol. 46, p. 457
