3,4-二氢-1-苯基萘合成路线 （共 70 条）
反应条件
NiCl2((PPh3)P)2 in diethyl ether; benzene
Ambient temperature;
参考文献
Ni, Zhi-Jie; Luh, Tien-Yau
Journal of the Chemical Society, Chemical Communications, 1987 , # 20 p. 1515 - 1517
反应条件
pyridine in methanol
T=5°C; 2 h; Irradiation;
参考文献
Kitamura, Tsugio; Muta, Tomonobu; Tahara, Toru; Kobayashi, Shinjiro; Taniguchi, Hiroshi
Chemistry Letters, 1986 , p. 759 - 762
参考文献
Cosmo, Robert; Sternhell, Sever
Australian Journal of Chemistry, 1987 , vol. 40, # 6 p. 1107 - 1126
反应条件
[RuCl2(cod)]n in 1,4-dioxane
T=120°C; 48 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Kozhushkov, Sergei I.; Yufit, Dmitry S.
Chemistry - A European Journal, 2012 , vol. 18, # 38 p. 12068 - 12077
反应条件
T=450°C; P=0.05 Torr;
参考文献
Harpp, David N.; Mullins, Dennis F.
Canadian Journal of Chemistry, 1983 , vol. 61, p. 757 - 761
反应条件
1.1: lithium / diethyl ether / 0.33 h / 20 °C / Inert atmosphere
1.2: 1 h / 20 °C / Inert atmosphere
2.1: toluene-4-sulfonic acid / benzene / 2 h / Reflux
View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
反应条件
1.1: methanesulfonic acid / 0.5 h / 90 °C / Inert atmosphere
2.1: lithium / diethyl ether / 0.33 h / 20 °C / Inert atmosphere
2.2: 1 h / 20 °C / Inert atmosphere
3.1: toluene-4-sulfonic acid / benzene / 2 h / Reflux
View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
反应条件
1.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C
1.2: 120 - 215 °C
2.1: methanesulfonic acid / 0.5 h / 90 °C / Inert atmosphere
3.1: lithium / diethyl ether / 0.33 h / 20 °C / Inert atmosphere
3.2: 1 h / 20 °C / Inert atmosphere
4.1: toluene-4-sulfonic acid / benzene / 2 h / Reflux
View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
反应条件
1.1: AlCl3, aluminium chloride / tetrachloroethane, 1,1,2,2-
2.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C
2.2: 120 - 215 °C
3.1: methanesulfonic acid / 0.5 h / 90 °C / Inert atmosphere
4.1: lithium / diethyl ether / 0.33 h / 20 °C / Inert atmosphere
4.2: 1 h / 20 °C / Inert atmosphere
5.1: toluene-4-sulfonic acid / benzene / 2 h / Reflux
View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
反应条件
1: trifluorormethanesulfonic acid / dichloromethane / 0.08 h / 20 °C
2: [1,3-bis(diphenylphosphino) propane] dichloronickel(II) / tetrahydrofuran / 1 h / 20 - 70 °C
View Scheme
参考文献
Eom, Dahan; Park, Sangjune; Park, Youngchul; Lee, Kooyeon; Hong, Gilbert; Lee, Phil Ho
European Journal of Organic Chemistry, 2013 , # 13 p. 2672 - 2682
