反应条件
1: NaBH4 / methanol / 0.08 h / 0 °C 2: 0.3 M aq. NaIO4 / tetrahydrofuran / 17 h / 23 °C 3: 2.) H2O / 1.) ether, -78 deg C, 10 min, 2.) ether, 23 deg C, 4 h 4: trifluoroacetic acid / CH2Cl2 / 24 h / 23 °C View Scheme
参考文献
Synthetic Communications, , vol. 24, # 6 p. 859 - 869