环己基-(4-甲氧基-苯基)-甲酮合成路线 (共 19 条)
反应条件
bis(1,5-cyclooctadiene)nickel (0); di-tert-butyl dicarbonate; bathophenanthroline; magnesium chloride; zinc in acetonitrile
T=25°C; 12 h; Inert atmosphere;
参考文献
Yin, Hongyu; Zhao, Chenglong; You, Hengzhi; Lin, Kunhua; Gong, Hegui
Chemical Communications, 2012 , vol. 48, # 56 p. 7034 - 7036
反应条件
bis(1,5-cyclooctadiene)nickel (0); bathophenanthroline; magnesium chloride; zinc in acetonitrile
T=25°C; 12 h; Inert atmosphere;
参考文献
Yin, Hongyu; Zhao, Chenglong; You, Hengzhi; Lin, Kunhua; Gong, Hegui
Chemical Communications, 2012 , vol. 48, # 56 p. 7034 - 7036
反应条件
1: 67 percent Chromat. / methyl vinyl ketone / Ru3(CO)12 / acetone; dioxane / 1 h / Heating
2: aq. HCl / tetrahydrofuran / 12 h
View Scheme
参考文献
Park, Young Jun; Jo, Eun-Ae; Jun, Chul-Ho
Chemical Communications, 2005 , # 9 p. 1185 - 1187
反应条件
tetrachlorosilane; p-trifluoromethylthiobenzoic anhydride; silver perchlorate in dichloromethane
25 h; Ambient temperature;
参考文献
Mukaiyama, Teruaki; Suzuki, Kaoru
Chemistry Letters, 1992 , # 9 p. 1751 - 1754
反应条件
[rhenium(pentacarbonyl)(bromide)] in 1,2-dichloro-ethane
2 h; Heating;
参考文献
Kusama, Hiroyuki; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 8 p. 2379 - 2384
反应条件
Cu(I) 3-methylsalicylate in N,N-dimethyl-formamide
1 h; Microwave irradiationHeatingInert atmosphereSealed tube;
参考文献
Zhang, Zhihui; Lindale, Matthew G.; Liebeskind, Lanny S.
Journal of the American Chemical Society, 2011 , vol. 133, # 16 p. 6403 - 6410
反应条件
1: 85 percent / LDA / tetrahydrofuran / 1 h / Ambient temperature
2: 26 percent / 9,10-dicyanoanthracene / acetonitrile / 113 h / Irradiation
View Scheme
参考文献
Ackermann, Lutz; Heidbreder, Andreas; Wurche, Frank; Klaerner, Frank-Gerrit; Mattay, Jochen
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 4 p. 863 - 869
反应条件
trimethylphenylammonium monobromide
参考文献
Marquet; Jacques
Tetrahedron Letters, 1959 , # 9 p. 24
Bulletin de la Societe Chimique de France, 1962 , p. 90,94
反应条件
sodium tetrahydroborate
参考文献
Shailaja; Kaanumalle, Lakshmi S.; Sivasubramanian, Karthikeyan; Natarajan, Arunkumar; Ponchot, Keith J.; Pradhan, Ajit; Ramamurthy
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 8 p. 1561 - 1571