反应条件
in diethyl ether
under dry nitrogen, addn. of a suspn. of CH3MgI to a soln. of B-compound, refluxing for 1 h; cooling, addn. of an aq. soln. of NH4Cl, filtn., washing (Et2O), drying organic layers (CaCl2), evapn. to dryness under reduced pressure;
参考文献
Allaoud, Smaiel; Conte, Seny; Fenet, Bernard; Frange, Bernard; Robert, Francis; et al.
Journal of Organometallic Chemistry, 1994 , vol. 469, # 1 p. 59 - 68
