(1Z)-1-[(羟基氨基)亚甲基]萘-2-酮合成路线 （共 13 条）
反应条件
toluene-4-sulfonic acid; triethylamine in dichloromethane T=20°C; 0.25 h;
参考文献
Dale, Trevor J.; Sather, Aaron C.; Rebek Jr., Julius
Tetrahedron Letters, 2009 , vol. 50, # 45 p. 6173 - 6175
反应条件
oxygen; benzaldehyde in toluene 4.41667 h; Reflux;
参考文献
Habibi; Faraji; Arshadi; Veisi; Gil
Journal of Molecular Catalysis A: Chemical, 2014 , vol. 382, p. 41 - 54
反应条件
hydroxylamine hydrochloride in ethanol
T=20 - 65°C;
参考文献
Dale, Trevor J.; Sather, Aaron C.; Rebek Jr., Julius
Tetrahedron Letters, 2009 , vol. 50, # 45 p. 6173 - 6175
反应条件
methanecarbohydroxamic acid; sulfuric acid in acetonitrile
T=80°C; P=1292.9 Torr; 0.2 h; Microwave irradiation;
参考文献
Madabhushi, Sridhar; Chinthala, Narsaiah; Vangipuram, Venkata Sairam; Godala, Kondal Reddy; Jillella, Raveendra; Mallu, Kishore Kumar Reddy; Beeram, China Ramanaiah
Tetrahedron Letters, 2011 , vol. 52, # 46 p. 6103 - 6107
反应条件
1: tetrabutylammomium bromide; sodium hydroxide / 1,4-dioxane / 2.08 h / 70 °C
2: hydroxylamine hydrochloride / dimethyl sulfoxide / 0.33 h / 20 °C
View Scheme
参考文献
Aspinall, Helen C.; Beckingham, Oliver; Farrar, Michael D.; Greeves, Nicholas; Thomas, Christopher D.
Tetrahedron Letters, 2011 , vol. 52, # 40 p. 5120 - 5123
反应条件
potassium carbonate in acetone
12 h; Heating;
参考文献
Ramesh; Chandrashekhar; Vaidya
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2008 , vol. 47, # 5 p. 753 - 758
反应条件
ammonium formate; palladium on activated charcoal in methanol
T=20°C; 16 h;
参考文献
Searcey, Mark; Grewal, Sukhwant S.; Madeo, Fiorenza; Tsoungas, Petros G.
Tetrahedron Letters, 2003 , vol. 44, # 35 p. 6745 - 6747
反应条件
hydrogen; platinum(IV) oxide in acetic acid
P=3000.3 Torr; Product distribution / selectivity;
参考文献
Exposito, Miriam Royo; Clauzel, Luc Marti; Martin, Anna Abella; Vicente, Silvia Garcia; Yinbert, Xavier Testar; Olarte, Antonio Zorzano; Prieto, Manuel Palacin; Palomera, Fernando Albericio; Font, Francesc Yraola; Mian, Alec
Patent: US2007/66682 A1, 2007 ;
Location in patent: Page/Page column 17 ;
反应条件
3: dioxane; aqueous H2SO4 / Hydrolysis
View Scheme
参考文献
Chauvellier
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1951 , vol. 232, p. 2458
反应条件
potassium carbonate in acetone
8 h; Heating;
参考文献
Ramesh; Chandrashekhar; Vaidya
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2008 , vol. 47, # 5 p. 753 - 758
